MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Summary Report Surface Area Single point surface area at p/p° = 0.300000000: 1,253.8138 m²/g BET Surface Area: 1,388.5063 m²/g Langmuir Surface Area: 2,371.6416 m²/g t-Plot Micropore Area: 833.7258 m²/g t-Plot External Surface Area: 554.7805 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 702.395 Å width: 602.465 m²/g BJH Desorption cumulative surface area of pores between 17.000 Å and 3,000.000 Å width: 650.7394 m²/g D-H Adsorption cumulative surface area of pores between 17.000 Å and 3,000.000 Å width: 584.685 m²/g D-H Desorption cumulative surface area of pores between 17.000 Å and 3,000.000 Å width: 630.9432 m²/g Pore Volume Single point adsorption total pore volume of pores less than 1,952.692 Å width at p/p° = 0.990093686: 0.795371 cm³/g t-Plot micropore volume: 0.347585 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 702.395 Å width: 0.451404 cm³/g BJH Desorption cumulative volume of pores between 17.000 Å and 3,000.000 Å width: 0.467240 cm³/g Pore Size Adsorption average pore diameter (4V/A by BET): 22.9130 Å BJH Adsorption average pore width (4V/A): 29.971 Å BJH Desorption average pore width (4V/A): 28.721 Å D-H Adsorption average pore width (4V/A): 30.173 Å D-H Desorption average pore width (4V/A): 28.907 Å Freundlich Qm·C: 0.44879 ± 0.1764 mmol/g m: 5.2763 ± 0.2352 Temkin q·alpha/Qm: 0.368754 ± 0.010719 kJ/mol·(mmol/g) A: 1686.8883 ± 433.1998 kPa DFT Pore Size Volume in Pores < 5.00 Å : 0.00000 cm³/g Total Volume in Pores <= 100.61 Å : 0.60196 cm³/g Area in Pores > 100.61 Å : 53.443 m²/g Total Area in Pores >= 5.00 Å : 945.076 m²/g DFT Surface Energy Total Area : 1,143.972 m²/g Nanoparticle Size: Average Particle Size 43.212 Å Horvath-Kawazoe Maximum pore volume at p/p° = 0.215438416: 0.594308 cm³/g Median pore width: 5.926 Å Dubinin-Astakhov Micropore surface area: 1,209.5693 m²/g Limiting micropore volume: 0.519766 cm³/g MP-Method Cumulative surface area of pores between 2.6231 Å and 19.2000 Å hydraulic radius: 1,429.4464 m²/g Cumulative pore volume of pores between 2.6231 Å and 19.2000 Å hydraulic radius: 0.784713 cm³/g Average pore hydraulic radius (V/A): 5.4896 Å MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Isotherm Tabular Report Relative Absolute Quantity Elapsed Saturation Pressure Pressure Adsorbed Time Pressure (p/p°) (kPa) (mmol/g) (h:min) (kPa) ----- 03:05 102.7167067 0.000007350 0.0007552 0.70286 03:31 102.7495572 0.000004304 0.0004421 1.40582 03:53 102.7106607 0.000005367 0.0005512 2.10930 04:13 102.6908707 0.000010131 0.0010401 2.81252 04:30 102.6666864 0.000019858 0.0020386 3.51431 04:45 102.6543177 0.000036792 0.0037762 4.21632 05:00 102.6371397 0.000064428 0.0066113 4.91536 05:13 102.6159744 0.000109592 0.0112449 5.61026 05:26 102.6074546 0.000185348 0.0190148 6.30345 05:41 102.5894548 0.000315239 0.0323360 6.98576 05:54 102.5761258 0.000542904 0.0556863 7.65352 06:09 102.5710400 0.000957593 0.0982205 8.31637 06:25 102.5702181 0.001749257 0.1794248 8.99069 06:40 102.5720002 0.001909516 0.1958526 9.09089 06:46 102.5666458 0.002878424 0.2952489 9.52252 06:51 102.5730987 0.003924408 0.4025139 9.85419 06:57 102.5667841 0.004805697 0.4929372 10.07242 07:02 102.5735137 0.005894287 0.6046204 10.29603 07:06 102.5773627 0.006778614 0.6954571 10.45226 07:10 102.5957775 0.007823680 0.8027227 10.61719 07:14 102.6016853 0.008962605 0.9195131 10.77887 07:18 102.5944023 0.010017462 1.0278828 10.91340 07:22 102.6091065 0.043712000 4.4854954 13.16695 07:31 102.6147376 0.077115042 7.9139776 14.42421 07:39 102.6256009 0.118862359 12.2007217 15.52855 07:46 102.6457978 0.144477242 14.8285122 16.05035 07:51 102.6356262 0.179663247 18.4400487 16.64080 07:56 102.6367328 0.215438416 22.1138481 17.14180 08:00 102.6457978 0.251250961 25.7926175 17.58196 08:04 102.6567914 0.284318380 29.1886586 17.95748 08:08 102.6618773 0.317050664 32.5461835 18.31262 08:12 102.6529424 0.349420429 35.8729249 18.65327 08:16 102.6640743 0.380226130 39.0363495 18.97272 08:19 102.6661412 0.413837781 42.4877511 19.31469 08:23 102.6676466 0.447562146 45.9543369 19.65223 08:27 102.6769965 0.481515038 49.4419049 19.99045 08:31 102.6798771 0.515462453 52.9326505 20.32592 08:35 102.6896338 0.549542896 56.4300200 20.65451 08:39 102.6853779 0.583502640 59.9175880 20.97212 08:42 102.6860615 0.617802380 63.4421565 21.26996 08:46 102.6900488 0.651981653 66.9549829 21.53731 08:49 102.6945813 0.686310950 70.4828674 21.76884 08:52 102.6981536 0.720674979 74.0151624 21.95851 08:55 102.7025559 0.754872074 77.5322730 22.11226 08:58 102.7091553 0.789285770 81.0687180 22.23565 09:00 102.7114907 0.823485965 84.5836153 22.33697 09:02 102.7140947 0.857677057 88.0997658 22.42427 09:04 102.7190422 0.891764700 91.6073476 22.50357 09:06 102.7259182 0.925734238 95.0990616 22.58535 09:07 102.7282537 0.959198444 98.5365157 22.69296 09:09 102.7279770 0.990093686 101.7218909 22.94111 09:12 102.7396622 0.947563232 97.3570144 22.76545 09:14 102.7446097 0.911482233 93.6546407 22.66519 09:16 102.7498258 0.876642619 90.0798199 22.59634 09:18 102.7554650 0.860242250 88.3927024 22.56465 09:19 102.7532679 0.825979307 84.8838755 22.51041 09:21 102.7675571 0.792364185 81.4335807 22.45758 09:22 102.7729196 0.758217753 77.9273741 22.40223 09:24 102.7770371 0.724294553 74.4392568 22.34401 09:26 102.7748400 0.690289213 70.9507164 22.28102 09:28 102.7840433 0.656450148 67.4735032 22.20973 09:29 102.7854186 0.622680280 64.0030562 22.12387 09:32 102.7863869 0.588832046 60.5266689 22.01992 09:34 102.7910577 0.555295374 57.0802393 21.88828 09:37 102.7925713 0.521545336 53.6066106 21.72606 09:39 102.7841817 0.488501340 50.2145751 21.51197 09:43 102.7931165 0.452664547 46.5399456 20.44068 09:59 102.8133215 0.423690887 43.5546029 19.64901 10:06 102.7980640 0.387932625 39.8761122 19.12743 10:12 102.7913344 0.337573066 34.7000474 18.58645 10:17 102.7927015 0.320056195 32.8991779 18.39728 10:20 102.7918796 0.284853985 29.2829481 18.01325 10:24 102.7998542 0.251037619 25.8069738 17.62706 10:28 102.8012213 0.217016955 22.3113987 17.20685 10:32 102.8094726 0.183392994 18.8554443 16.74038 10:37 102.8144201 0.149791193 15.4015588 16.18866 10:41 102.8201895 0.116281004 11.9567862 15.50913 10:47 102.8266505 0.078188298 8.0396041 14.49203 10:54 102.8236234 0.044689266 4.5951061 13.24494 11:02 102.8234851 0.010161999 1.0448629 10.96703 11:17 102.8206045 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Isotherm Linear Plot ACF 1 - Adsorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.34981e-006 0.702863 4.30389e-006 1.40582 5.36731e-006 2.1093 1.01313e-005 2.81252 1.98585e-005 3.51431 3.67919e-005 4.21632 6.44276e-005 4.91536 0.000109592 5.61026 0.000185348 6.30345 0.000315239 6.98576 0.000542904 7.65352 0.000957593 8.31637 0.00174926 8.99069 0.00190952 9.09089 0.00287842 9.52252 0.00392441 9.85419 0.0048057 10.0724 0.00589429 10.296 0.00677861 10.4523 0.00782368 10.6172 0.0089626 10.7789 0.0100175 10.9134 0.043712 13.1669 0.077115 14.4242 0.118862 15.5285 0.144477 16.0504 0.179663 16.6408 0.215438 17.1418 0.251251 17.582 0.284318 17.9575 0.317051 18.3126 0.34942 18.6533 0.380226 18.9727 0.413838 19.3147 0.447562 19.6522 0.481515 19.9905 0.515462 20.3259 0.549543 20.6545 0.583503 20.9721 0.617802 21.27 0.651982 21.5373 0.686311 21.7688 0.720675 21.9585 0.754872 22.1123 0.789286 22.2357 0.823486 22.337 0.857677 22.4243 0.891765 22.5036 0.925734 22.5854 0.959198 22.693 0.990094 22.9411 ACF 1 - Desorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 0.990094 22.9411 0.947563 22.7655 0.911482 22.6652 0.876643 22.5963 0.860242 22.5646 0.825979 22.5104 0.792364 22.4576 0.758218 22.4022 0.724295 22.344 0.690289 22.281 0.65645 22.2097 0.62268 22.1239 0.588832 22.0199 0.555295 21.8883 0.521545 21.7261 0.488501 21.512 0.452665 20.4407 0.423691 19.649 0.387933 19.1274 0.337573 18.5864 0.320056 18.3973 0.284854 18.0133 0.251038 17.6271 0.217017 17.2069 0.183393 16.7404 0.149791 16.1887 0.116281 15.5091 0.0781883 14.492 0.0446893 13.2449 0.010162 10.967 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Isotherm Log Plot ACF 1 - Adsorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.34981e-006 0.702863 4.30389e-006 1.40582 5.36731e-006 2.1093 1.01313e-005 2.81252 1.98585e-005 3.51431 3.67919e-005 4.21632 6.44276e-005 4.91536 0.000109592 5.61026 0.000185348 6.30345 0.000315239 6.98576 0.000542904 7.65352 0.000957593 8.31637 0.00174926 8.99069 0.00190952 9.09089 0.00287842 9.52252 0.00392441 9.85419 0.0048057 10.0724 0.00589429 10.296 0.00677861 10.4523 0.00782368 10.6172 0.0089626 10.7789 0.0100175 10.9134 0.043712 13.1669 0.077115 14.4242 0.118862 15.5285 0.144477 16.0504 0.179663 16.6408 0.215438 17.1418 0.251251 17.582 0.284318 17.9575 0.317051 18.3126 0.34942 18.6533 0.380226 18.9727 0.413838 19.3147 0.447562 19.6522 0.481515 19.9905 0.515462 20.3259 0.549543 20.6545 0.583503 20.9721 0.617802 21.27 0.651982 21.5373 0.686311 21.7688 0.720675 21.9585 0.754872 22.1123 0.789286 22.2357 0.823486 22.337 0.857677 22.4243 0.891765 22.5036 0.925734 22.5854 0.959198 22.693 0.990094 22.9411 ACF 1 - Desorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 0.990094 22.9411 0.947563 22.7655 0.911482 22.6652 0.876643 22.5963 0.860242 22.5646 0.825979 22.5104 0.792364 22.4576 0.758218 22.4022 0.724295 22.344 0.690289 22.281 0.65645 22.2097 0.62268 22.1239 0.588832 22.0199 0.555295 21.8883 0.521545 21.7261 0.488501 21.512 0.452665 20.4407 0.423691 19.649 0.387933 19.1274 0.337573 18.5864 0.320056 18.3973 0.284854 18.0133 0.251038 17.6271 0.217017 17.2069 0.183393 16.7404 0.149791 16.1887 0.116281 15.5091 0.0781883 14.492 0.0446893 13.2449 0.010162 10.967 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Isotherm Linear Absolute Plot ACF 1 - Adsorption Absolute Pressure (kPa) Quantity Adsorbed (mmol/g) 0.00075519 0.702863 0.000442056 1.40582 0.000551174 2.1093 0.00104015 2.81252 0.00203856 3.51431 0.00377621 4.21632 0.0066113 4.91536 0.0112449 5.61026 0.0190148 6.30345 0.032336 6.98576 0.0556863 7.65352 0.0982205 8.31637 0.179425 8.99069 0.195853 9.09089 0.295249 9.52252 0.402514 9.85419 0.492937 10.0724 0.60462 10.296 0.695457 10.4523 0.802723 10.6172 0.919513 10.7789 1.02788 10.9134 4.4855 13.1669 7.91398 14.4242 12.2007 15.5285 14.8285 16.0504 18.44 16.6408 22.1138 17.1418 25.7926 17.582 29.1887 17.9575 32.5462 18.3126 35.8729 18.6533 39.0363 18.9727 42.4878 19.3147 45.9543 19.6522 49.4419 19.9905 52.9327 20.3259 56.43 20.6545 59.9176 20.9721 63.4422 21.27 66.955 21.5373 70.4829 21.7688 74.0152 21.9585 77.5323 22.1123 81.0687 22.2357 84.5836 22.337 88.0998 22.4243 91.6073 22.5036 95.0991 22.5854 98.5365 22.693 101.722 22.9411 ACF 1 - Desorption Absolute Pressure (kPa) Quantity Adsorbed (mmol/g) 101.722 22.9411 97.357 22.7655 93.6546 22.6652 90.0798 22.5963 88.3927 22.5646 84.8839 22.5104 81.4336 22.4576 77.9274 22.4022 74.4393 22.344 70.9507 22.281 67.4735 22.2097 64.0031 22.1239 60.5267 22.0199 57.0802 21.8883 53.6066 21.7261 50.2146 21.512 46.5399 20.4407 43.5546 19.649 39.8761 19.1274 34.7 18.5864 32.8992 18.3973 29.2829 18.0133 25.807 17.6271 22.3114 17.2069 18.8554 16.7404 15.4016 16.1887 11.9568 15.5091 8.0396 14.492 4.59511 13.2449 1.04486 10.967 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Isotherm Log Absolute Plot ACF 1 - Adsorption Absolute Pressure (kPa) Quantity Adsorbed (mmol/g) 0.00075519 0.702863 0.000442056 1.40582 0.000551174 2.1093 0.00104015 2.81252 0.00203856 3.51431 0.00377621 4.21632 0.0066113 4.91536 0.0112449 5.61026 0.0190148 6.30345 0.032336 6.98576 0.0556863 7.65352 0.0982205 8.31637 0.179425 8.99069 0.195853 9.09089 0.295249 9.52252 0.402514 9.85419 0.492937 10.0724 0.60462 10.296 0.695457 10.4523 0.802723 10.6172 0.919513 10.7789 1.02788 10.9134 4.4855 13.1669 7.91398 14.4242 12.2007 15.5285 14.8285 16.0504 18.44 16.6408 22.1138 17.1418 25.7926 17.582 29.1887 17.9575 32.5462 18.3126 35.8729 18.6533 39.0363 18.9727 42.4878 19.3147 45.9543 19.6522 49.4419 19.9905 52.9327 20.3259 56.43 20.6545 59.9176 20.9721 63.4422 21.27 66.955 21.5373 70.4829 21.7688 74.0152 21.9585 77.5323 22.1123 81.0687 22.2357 84.5836 22.337 88.0998 22.4243 91.6073 22.5036 95.0991 22.5854 98.5365 22.693 101.722 22.9411 ACF 1 - Desorption Absolute Pressure (kPa) Quantity Adsorbed (mmol/g) 101.722 22.9411 97.357 22.7655 93.6546 22.6652 90.0798 22.5963 88.3927 22.5646 84.8839 22.5104 81.4336 22.4576 77.9274 22.4022 74.4393 22.344 70.9507 22.281 67.4735 22.2097 64.0031 22.1239 60.5267 22.0199 57.0802 21.8883 53.6066 21.7261 50.2146 21.512 46.5399 20.4407 43.5546 19.649 39.8761 19.1274 34.7 18.5864 32.8992 18.3973 29.2829 18.0133 25.807 17.6271 22.3114 17.2069 18.8554 16.7404 15.4016 16.1887 11.9568 15.5091 8.0396 14.492 4.59511 13.2449 1.04486 10.967 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Isotherm Pressure Composition ACF 1 - Adsorption Weight % N2 Absolute Pressure (kPa) 1.96872 0.00075519 3.9377 0.000442056 5.90816 0.000551174 7.87787 0.00104015 9.84359 0.00203856 11.8099 0.00377621 13.7679 0.0066113 15.7143 0.0112449 17.656 0.0190148 19.5671 0.032336 21.4375 0.0556863 23.2942 0.0982205 25.1829 0.179425 25.4636 0.195853 26.6726 0.295249 27.6016 0.402514 28.2129 0.492937 28.8392 0.60462 29.2768 0.695457 29.7387 0.802723 30.1916 0.919513 30.5684 1.02788 36.8806 4.4855 40.4022 7.91398 43.4955 12.2007 44.957 14.8285 46.6109 18.44 48.0142 22.1138 49.2471 25.7926 50.2989 29.1887 51.2937 32.5462 52.2478 35.8729 53.1426 39.0363 54.1005 42.4878 55.0459 45.9543 55.9933 49.4419 56.9329 52.9327 57.8533 56.43 58.7429 59.9176 59.5772 63.4422 60.326 66.955 60.9745 70.4829 61.5058 74.0152 61.9365 77.5323 62.2821 81.0687 62.5658 84.5836 62.8104 88.0998 63.0325 91.6073 63.2616 95.0991 63.563 98.5365 64.258 101.722 ACF 1 - Desorption Weight % N2 Absolute Pressure (kPa) 64.258 101.722 63.766 97.357 63.4852 93.6546 63.2923 90.0798 63.2036 88.3927 63.0517 84.8839 62.9037 81.4336 62.7486 77.9274 62.5856 74.4393 62.4091 70.9507 62.2094 67.4735 61.969 64.0031 61.6778 60.5267 61.3091 57.0802 60.8547 53.6066 60.255 50.2146 57.2544 46.5399 55.0369 43.5546 53.5759 39.8761 52.0606 34.7 51.5308 32.8992 50.4551 29.2829 49.3734 25.807 48.1964 22.3114 46.8898 18.8554 45.3444 15.4016 43.4411 11.9568 40.5922 8.0396 37.0991 4.59511 30.7187 1.04486 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BET Report BET Surface Area: 1388.5063 ± 6.1132 m²/g Slope: 0.069852 ± 0.000308 g/mmol Y-Intercept: 0.000410 ± 0.000032 g/mmol C: 171.557778 Qm: 14.23246 mmol/g Correlation Coefficient: 0.9999806 Molecular Cross-Sectional Area: 0.1620 nm² Relative Quantity Pressure Adsorbed 1/[Q(p°/p (p/p°) (mmol/g) - 1)] --- 0.043712000 13.16695 0.00347 0.077115042 14.42421 0.00579 0.118862359 15.52855 0.00869 0.144477242 16.05035 0.01052 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BET Surface Area Plot ACF 1 Relative Pressure (p/p°) 1/[Q(p°/p - 1)] 0.043712 0.00347158 0.077115 0.00579295 0.118862 0.008687 0.144477 0.0105216 Not Fitted Relative Pressure (p/p°) 1/[Q(p°/p - 1)] 0.179663 0.0131611 0.215438 0.0160192 0.251251 0.0190855 0.284318 0.0221228 0.317051 0.0253507 0.34942 0.0287934 0.380226 0.0323355 0.413838 0.0365531 0.447562 0.0412248 0.481515 0.046457 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Langmuir Report Langmuir Surface Area: 2,371.6416 ± 31.4380 m²/g Slope: 0.04114 ± 0.00055 g/mmol Y-Intercept: 0.358 ± 0.031 kPa·g/mmol b: 0.11476 1/kPa Qm: 24.30979 mmol/g Correlation Coefficient: 0.997811 Molecular Cross-Sectional Area: 0.1620 nm² Quantity Pressure Adsorbed p/Q (kPa) (mmol/g) (kPa·g/mmol) --- 4.4854954 13.16695 0.341 7.9139776 14.42421 0.549 12.2007217 15.52855 0.786 14.8285122 16.05035 0.924 18.4400487 16.64080 1.108 22.1138481 17.14180 1.290 25.7926175 17.58196 1.467 29.1886586 17.95748 1.625 32.5461835 18.31262 1.777 35.8729249 18.65327 1.923 39.0363495 18.97272 2.057 42.4877511 19.31469 2.200 45.9543369 19.65223 2.338 49.4419049 19.99045 2.473 52.9326505 20.32592 2.604 56.4300200 20.65451 2.732 59.9175880 20.97212 2.857 63.4421565 21.26996 2.983 66.9549829 21.53731 3.109 70.4828674 21.76884 3.238 74.0151624 21.95851 3.371 77.5322730 22.11226 3.506 81.0687180 22.23565 3.646 84.5836153 22.33697 3.787 88.0997658 22.42427 3.929 91.6073476 22.50357 4.071 95.0990616 22.58535 4.211 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Langmuir Surface Area Plot ACF 1 Pressure (kPa) p/Q (kPa·g/mmol) 4.4855 0.340663 7.91398 0.548659 12.2007 0.785696 14.8285 0.923875 18.44 1.10812 22.1138 1.29005 25.7926 1.46699 29.1887 1.62543 32.5462 1.77725 35.8729 1.92314 39.0363 2.0575 42.4878 2.19976 45.9543 2.33838 49.4419 2.47328 52.9327 2.60419 56.43 2.73209 59.9176 2.85701 63.4422 2.98271 66.955 3.10879 70.4829 3.23779 74.0152 3.37068 77.5323 3.5063 81.0687 3.64589 84.5836 3.78671 88.0998 3.92877 91.6073 4.07079 95.0991 4.21065 Not Fitted Pressure (kPa) p/Q (kPa·g/mmol) 98.5365 4.34216 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Freundlich Tabular Report Qm·C: 10.0592 ± 0.1764 mmol/g m: 5.2763 ± 0.2352 Correlation Coefficient: 0.954602 Absolute Quantity Pressure Adsorbed (kPa) (mmol/g) log(p) log(Q) ---- 0.0007552 0.70286 -3.12194 -0.1531 0.0004421 1.40582 -3.35452 0.1479 0.0005512 2.10930 -3.25871 0.3241 0.0010401 2.81252 -2.98291 0.4491 0.0020386 3.51431 -2.69068 0.5458 0.0037762 4.21632 -2.42294 0.6249 0.0066113 4.91536 -2.17971 0.6916 0.0112449 5.61026 -1.94904 0.7490 0.0190148 6.30345 -1.72091 0.7996 0.0323360 6.98576 -1.49031 0.8442 0.0556863 7.65352 -1.25425 0.8839 0.0982205 8.31637 -1.00780 0.9199 0.1794248 8.99069 -0.74612 0.9538 0.1958526 9.09089 -0.70807 0.9586 0.2952489 9.52252 -0.52981 0.9788 0.4025139 9.85419 -0.39522 0.9936 0.4929372 10.07242 -0.30721 1.0031 0.6046204 10.29603 -0.21852 1.0127 0.6954571 10.45226 -0.15773 1.0192 0.8027227 10.61719 -0.09543 1.0260 0.9195131 10.77887 -0.03644 1.0326 1.0278828 10.91340 0.01194 1.0380 4.4854954 13.16695 0.65181 1.1195 7.9139776 14.42421 0.89839 1.1591 12.2007217 15.52855 1.08639 1.1911 14.8285122 16.05035 1.17110 1.2055 18.4400487 16.64080 1.26576 1.2212 22.1138481 17.14180 1.34466 1.2341 25.7926175 17.58196 1.41150 1.2451 29.1886586 17.95748 1.46521 1.2542 32.5461835 18.31262 1.51250 1.2628 35.8729249 18.65327 1.55477 1.2708 39.0363495 18.97272 1.59147 1.2781 42.4877511 19.31469 1.62826 1.2859 45.9543369 19.65223 1.66233 1.2934 49.4419049 19.99045 1.69410 1.3008 52.9326505 20.32592 1.72372 1.3081 56.4300200 20.65451 1.75151 1.3150 59.9175880 20.97212 1.77755 1.3216 63.4421565 21.26996 1.80238 1.3278 66.9549829 21.53731 1.82578 1.3332 70.4828674 21.76884 1.84808 1.3378 74.0151624 21.95851 1.86932 1.3416 77.5322730 22.11226 1.88948 1.3446 81.0687180 22.23565 1.90885 1.3470 84.5836153 22.33697 1.92729 1.3490 88.0997658 22.42427 1.94497 1.3507 91.6073476 22.50357 1.96193 1.3523 95.0990616 22.58535 1.97818 1.3538 98.5365157 22.69296 1.99360 1.3559 101.7218909 22.94111 2.00741 1.3606 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Freundlich Plot ACF 1 log(p) log(Q) -3.12194 -0.153129 -3.35452 0.14793 -3.25871 0.324139 -2.98291 0.449095 -2.69068 0.545841 -2.42294 0.624934 -2.17971 0.691556 -1.94904 0.748983 -1.72091 0.799578 -1.49031 0.844213 -1.25425 0.883861 -1.0078 0.919934 -0.746118 0.953793 -0.708071 0.958607 -0.529812 0.978752 -0.395219 0.993621 -0.307208 1.00313 -0.218517 1.01267 -0.15773 1.01921 -0.0954344 1.02601 -0.0364421 1.03257 0.0119436 1.03796 0.65181 1.11949 0.898395 1.15909 1.08639 1.19113 1.1711 1.20548 1.26576 1.22117 1.34466 1.23406 1.4115 1.24507 1.46521 1.25425 1.5125 1.26275 1.55477 1.27075 1.59147 1.27813 1.62826 1.28589 1.66233 1.29341 1.6941 1.30082 1.72372 1.30805 1.75151 1.31501 1.77755 1.32164 1.80238 1.32777 1.82578 1.33319 1.84808 1.33784 1.86932 1.3416 1.88948 1.34463 1.90885 1.34705 1.92729 1.34902 1.94497 1.35072 1.96193 1.35225 1.97818 1.35383 1.9936 1.35589 2.00741 1.36061 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Temkin Tabular Report q·alpha/Qm: 0.368754 ± 0.010719 kJ/mol·(mmol/g) A: 1686.8883 ± 433.1998 1/kPa Correlation Coefficient: 0.979919 Absolute Quantity Pressure Adsorbed (kPa) (mmol/g) ln(p) --- 0.0007552 0.70286 -7.18854 0.0004421 1.40582 -7.72407 0.0005512 2.10930 -7.50346 0.0010401 2.81252 -6.86839 0.0020386 3.51431 -6.19551 0.0037762 4.21632 -5.57903 0.0066113 4.91536 -5.01898 0.0112449 5.61026 -4.48784 0.0190148 6.30345 -3.96254 0.0323360 6.98576 -3.43157 0.0556863 7.65352 -2.88802 0.0982205 8.31637 -2.32054 0.1794248 8.99069 -1.71800 0.1958526 9.09089 -1.63039 0.2952489 9.52252 -1.21994 0.4025139 9.85419 -0.91003 0.4929372 10.07242 -0.70737 0.6046204 10.29603 -0.50315 0.6954571 10.45226 -0.36319 0.8027227 10.61719 -0.21975 0.9195131 10.77887 -0.08391 1.0278828 10.91340 0.02750 4.4854954 13.16695 1.50085 7.9139776 14.42421 2.06863 12.2007217 15.52855 2.50150 14.8285122 16.05035 2.69655 18.4400487 16.64080 2.91452 22.1138481 17.14180 3.09620 25.7926175 17.58196 3.25009 29.1886586 17.95748 3.37378 32.5461835 18.31262 3.48266 35.8729249 18.65327 3.57998 39.0363495 18.97272 3.66449 42.4877511 19.31469 3.74922 45.9543369 19.65223 3.82765 49.4419049 19.99045 3.90080 52.9326505 20.32592 3.96902 56.4300200 20.65451 4.03300 59.9175880 20.97212 4.09297 63.4421565 21.26996 4.15013 66.9549829 21.53731 4.20402 70.4828674 21.76884 4.25537 74.0151624 21.95851 4.30427 77.5322730 22.11226 4.35069 81.0687180 22.23565 4.39530 84.5836153 22.33697 4.43774 88.0997658 22.42427 4.47847 91.6073476 22.50357 4.51751 95.0990616 22.58535 4.55492 98.5365157 22.69296 4.59043 101.7218909 22.94111 4.62224 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Temkin Plot ACF 1 ln(p) Quantity Adsorbed (mmol/g) -7.18854 0.702863 -7.72407 1.40582 -7.50346 2.1093 -6.86839 2.81252 -6.19551 3.51431 -5.57903 4.21632 -5.01898 4.91536 -4.48784 5.61026 -3.96254 6.30345 -3.43157 6.98576 -2.88802 7.65352 -2.32054 8.31637 -1.718 8.99069 -1.63039 9.09089 -1.21994 9.52252 -0.910026 9.85419 -0.707373 10.0724 -0.503155 10.296 -0.363186 10.4523 -0.219746 10.6172 -0.083911 10.7789 0.0275011 10.9134 1.50085 13.1669 2.06863 14.4242 2.5015 15.5285 2.69655 16.0504 2.91452 16.6408 3.0962 17.1418 3.25009 17.582 3.37378 17.9575 3.48266 18.3126 3.57998 18.6533 3.66449 18.9727 3.74922 19.3147 3.82765 19.6522 3.9008 19.9905 3.96902 20.3259 4.033 20.6545 4.09297 20.9721 4.15013 21.27 4.20402 21.5373 4.25537 21.7688 4.30427 21.9585 4.35069 22.1123 4.3953 22.2357 4.43774 22.337 4.47847 22.4243 4.51751 22.5036 4.55492 22.5854 4.59043 22.693 4.62224 22.9411 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No t-Plot Report Micropore Volume: 0.347585 cm³/g Micropore Area: 833.7258 m²/g External Surface Area: 554.7805 m²/g Slope: 1.600169 ± 0.046652 mmol/g·Å Y-Intercept: 10.025487 ± 0.246655 mmol/g Correlation Coefficient: 0.996617 Surface Area Correction Factor: 1.000 Density Conversion Factor: 0.0015468 Total Surface Area (BET): 1388.5063 m²/g Thickness Range: 4.0171 Å to 6.4783 Å Thickness Equation: Harkins and Jura Thickness Curve t = [ 13.99 / ( 0.034 - log(p/p°) ) ] ^ 0.5 t-Plot Report - Data Relative Statistical Quantity Pressure Thickness Adsorbed (p/p°) (Å) (mmol/g) Fitted --- 0.002878424 2.3310 9.52252 0.003924408 2.3944 9.85419 0.004805697 2.4388 10.07242 0.005894287 2.4861 10.29603 0.006778614 2.5201 10.45226 0.007823680 2.5565 10.61719 0.008962605 2.5925 10.77887 0.010017462 2.6231 10.91340 0.043712000 3.1686 13.16695 0.077115042 3.4926 14.42421 0.118862359 3.8195 15.52855 0.144477242 4.0004 16.05035 0.179663247 4.2363 16.64080 * 0.215438416 4.4684 17.14180 * 0.251250961 4.6979 17.58196 * 0.284318380 4.9105 17.95748 * 0.317050664 5.1239 18.31262 * 0.349420429 5.3398 18.65327 * 0.380226130 5.5514 18.97272 * 0.413837781 5.7910 19.31469 * 0.447562146 6.0426 19.65223 * 0.481515038 6.3098 19.99045 * 0.515462453 6.5935 20.32592 0.549542896 6.8982 20.65451 0.583502640 7.2256 20.97212 0.617802380 7.5853 21.26996 0.651981653 7.9787 21.53731 0.686310950 8.4168 21.76884 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No t-Plot Harkins and Jura ACF 1 Thickness (Å) Quantity Adsorbed (mmol/g) 4.23633 16.6408 4.46838 17.1418 4.69787 17.582 4.91046 17.9575 5.12386 18.3126 5.33977 18.6533 5.55138 18.9727 5.79098 19.3147 6.04263 19.6522 6.30978 19.9905 Not Fitted Thickness (Å) Quantity Adsorbed (mmol/g) 2.33095 9.52252 2.39438 9.85419 2.43875 10.0724 2.48606 10.296 2.52009 10.4523 2.55648 10.6172 2.59247 10.7789 2.6231 10.9134 3.16863 13.1669 3.49264 14.4242 3.81953 15.5285 4.0004 16.0504 6.59347 20.3259 6.89821 20.6545 7.22564 20.9721 7.58528 21.27 7.97866 21.5373 8.41683 21.7688 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BJH Adsorption Pore Distribution Report Faas Correction Harkins and Jura t = [ 13.99 / ( 0.034 - log(p/p°) ) ] ^ 0.5 Width Range: 17.000 Å to 702.395 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 1952.7 - 490.3 569.9 0.009685 0.009685 0.680 0.680 490.3 - 275.8 324.5 0.004338 0.014023 0.535 1.214 275.8 - 192.2 218.5 0.003433 0.017456 0.628 1.843 192.2 - 147.7 163.7 0.003488 0.020944 0.852 2.695 147.7 - 119.9 130.6 0.004034 0.024978 1.235 3.930 119.9 - 100.8 108.5 0.004905 0.029883 1.808 5.739 100.8 - 86.7 92.6 0.006247 0.036130 2.700 8.438 86.7 - 76.0 80.6 0.008125 0.044255 4.034 12.472 76.0 - 67.5 71.2 0.010399 0.054655 5.846 18.318 67.5 - 60.5 63.6 0.013134 0.067789 8.266 26.583 60.5 - 54.7 57.3 0.015584 0.083373 10.879 37.462 54.7 - 49.8 52.0 0.017744 0.101117 13.643 51.105 49.8 - 45.6 47.5 0.019259 0.120376 16.212 67.317 45.6 - 41.9 43.6 0.020141 0.140517 18.474 85.791 41.9 - 38.7 40.2 0.020754 0.161271 20.666 106.457 38.7 - 35.8 37.1 0.021026 0.182297 22.662 129.120 35.8 - 33.2 34.4 0.021037 0.203334 24.481 153.601 33.2 - 30.8 31.9 0.021403 0.224737 26.842 180.443 30.8 - 28.8 29.7 0.020046 0.244783 26.972 207.415 28.8 - 26.8 27.7 0.021356 0.266139 30.794 238.210 26.8 - 25.0 25.8 0.022303 0.288441 34.542 272.752 25.0 - 23.2 24.0 0.023675 0.312116 39.451 312.202 23.2 - 21.4 22.2 0.028150 0.340267 50.766 362.968 21.4 - 19.6 20.4 0.033046 0.373313 64.896 427.864 19.6 - 17.9 18.6 0.040697 0.414011 87.448 515.312 17.9 - 16.6 17.2 0.037394 0.451404 87.153 602.465 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BJH Adsorption Cumulative Pore Volume (Larger) Harkins and Jura : Faas Correction ACF 1 Pore Width (Å) Pore Volume (cm³/g) 490.319 0.00968534 275.783 0.0140234 192.235 0.017456 147.723 0.0209439 119.887 0.0249779 100.777 0.0298833 86.7114 0.0361305 76.0047 0.0442551 67.468 0.0546545 60.5172 0.0677887 54.7481 0.0833725 49.8323 0.101117 45.6337 0.120376 41.9485 0.140517 38.6999 0.161271 35.7935 0.182297 33.1851 0.203334 30.8134 0.224737 28.8064 0.244783 26.8405 0.266139 24.976 0.288441 23.1943 0.312116 21.353 0.340267 19.5755 0.373313 17.8528 0.414011 16.5883 0.451404 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BJH Adsorption dV/dw Pore Volume Harkins and Jura : Faas Correction ACF 1 Pore Width (Å) dV/dw Pore Volume (cm³/g·Å) 569.907 6.62303e-006 324.522 2.02206e-005 218.468 4.10849e-005 163.724 7.83591e-005 130.643 0.000144919 108.501 0.000256686 92.5653 0.000444162 80.5642 0.000758833 71.1597 0.0012182 63.5612 0.0018896 57.3005 0.00270123 52.0228 0.00360967 47.5181 0.004587 43.6096 0.00546525 40.1702 0.00638884 37.1126 0.00723449 34.372 0.00806488 31.8942 0.00902442 29.7287 0.00998787 27.7396 0.0108631 25.8269 0.011962 24.0048 0.0132878 22.1803 0.0152885 20.369 0.0185914 18.6156 0.0236236 17.1624 0.0295719 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BJH Desorption Pore Distribution Report Faas Correction Harkins and Jura t = [ 13.99 / ( 0.034 - log(p/p°) ) ] ^ 0.5 Width Range: 17.000 Å to 3,000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 1952.7 - 385.1 437.5 0.007062 0.007062 0.646 0.646 385.1 - 233.1 271.7 0.004161 0.011223 0.612 1.258 233.1 - 169.5 190.7 0.002948 0.014170 0.618 1.876 169.5 - 150.3 158.7 0.001396 0.015566 0.352 2.228 150.3 - 121.6 132.6 0.002427 0.017993 0.732 2.960 121.6 - 102.3 110.1 0.002455 0.020448 0.892 3.852 102.3 - 87.9 93.9 0.002671 0.023119 1.138 4.991 87.9 - 77.0 81.7 0.002914 0.026034 1.428 6.418 77.0 - 68.4 72.1 0.003267 0.029301 1.812 8.230 68.4 - 61.3 64.4 0.003847 0.033148 2.388 10.619 61.3 - 55.5 58.1 0.004840 0.037988 3.333 13.952 55.5 - 50.5 52.8 0.006093 0.044081 4.619 18.571 50.5 - 46.3 48.2 0.008051 0.052132 6.680 25.251 46.3 - 42.6 44.3 0.010251 0.062383 9.266 34.516 42.6 - 39.3 40.8 0.014111 0.076494 13.833 48.349 39.3 - 36.2 37.6 0.078838 0.155332 83.822 132.171 36.2 - 33.9 35.0 0.057453 0.212785 65.703 197.874 33.9 - 31.3 32.5 0.033727 0.246512 41.500 239.373 31.3 - 28.1 29.5 0.031088 0.277600 42.168 281.541 28.1 - 27.0 27.5 0.010765 0.288366 15.648 297.189 27.0 - 25.0 25.9 0.021823 0.310189 33.681 330.870 25.0 - 23.2 24.0 0.022145 0.332334 36.892 367.762 23.2 - 21.4 22.2 0.024651 0.356985 44.370 412.132 21.4 - 19.8 20.5 0.028396 0.385382 55.376 467.508 19.8 - 18.1 18.8 0.035512 0.420894 75.369 542.877 18.1 - 16.5 17.2 0.046346 0.467240 107.863 650.739 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BJH Desorption Cumulative Pore Volume (Larger) Harkins and Jura : Faas Correction ACF 1 Pore Width (Å) Pore Volume (cm³/g) 385.096 0.00706209 233.1 0.0112226 169.545 0.0141704 150.339 0.0155662 121.561 0.0179929 102.25 0.0204481 87.9119 0.0231194 77.0194 0.0260338 68.3656 0.0293007 61.3491 0.0331476 55.5128 0.0379878 50.5474 0.0440811 46.3047 0.0521318 42.5725 0.062383 39.3382 0.0764942 36.211 0.155332 33.9215 0.212785 31.3392 0.246512 28.0712 0.2776 27.0175 0.288366 25.0057 0.310189 23.1831 0.332334 21.4327 0.356985 19.759 0.385382 18.113 0.420894 16.4593 0.46724 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No BJH Desorption dV/dw Pore Volume Harkins and Jura : Faas Correction ACF 1 Pore Width (Å) dV/dw Pore Volume (cm³/g·Å) 437.495 4.50504e-006 271.742 2.73725e-005 190.726 4.63827e-005 158.681 7.26724e-005 132.627 8.43251e-005 110.063 0.000127141 93.8742 0.000186307 81.6557 0.000267561 72.1082 0.000377511 64.4239 0.000548258 58.0959 0.000829339 52.7613 0.00122714 48.2099 0.00189755 44.2553 0.00274667 40.8052 0.004363 37.6217 0.0252104 34.9774 0.0250943 32.5084 0.013061 29.4898 0.00951286 27.52 0.0102171 25.9172 0.0108472 24.0103 0.0121503 22.2236 0.0140831 20.5119 0.0169662 18.8471 0.0215755 17.1872 0.0280256 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Horvath-Kawazoe Report Slit Pore Geometry (Original H-K) Maximum pore volume: 0.594308 cm³/g at Relative Pressure: 0.215438416 Median pore width: 5.926 Å Relative pressure range: 7.350e-006 to 2.154e-001 Diameter of adsorptive molecule: 3.000 Å Diameter of adsorptive at zero interaction energy: 2.574 Å Adsorptive density: 6.710e+014 molecules/cm² Adsorptive dispersion constant: 7.777e-059 Diameter of sample atom: 3.400 Å Diameter of sample atom at zero interaction energy: 2.918 Å Sample Density: 3.845e+015 molecules/cm² Sample dispersion constant: 6.036e-059 Density conversion factor: 0.0015468 Cumulative Differential Absolute Relative Quantity Pore Pore Pore Pressure Pressure Adsorbed Width Volume Volume (kPa) (p/p°) (mmol/g) (Å) (cm³/g) (cm³/g·Å) ------ 0.00076 0.000007350 0.70286 3.999 0.0244 0.0061 0.00044 0.000004304 1.40582 3.866 0.0487 -0.1830 0.00055 0.000005367 2.10930 3.920 0.0731 0.4476 0.00104 0.000010131 2.81252 4.082 0.0975 0.1507 0.00204 0.000019858 3.51431 4.264 0.1218 0.1333 0.00378 0.000036792 4.21632 4.445 0.1462 0.1346 0.00661 0.000064428 4.91536 4.623 0.1704 0.1361 0.01124 0.000109592 5.61026 4.807 0.1945 0.1311 0.01901 0.000185348 6.30345 5.006 0.2185 0.1205 0.03234 0.000315239 6.98576 5.229 0.2422 0.1062 0.05569 0.000542904 7.65352 5.484 0.2653 0.0909 0.09822 0.000957593 8.31637 5.785 0.2883 0.0763 0.17942 0.001749257 8.99069 6.157 0.3117 0.0628 0.19585 0.001909516 9.09089 6.216 0.3152 0.0586 0.29525 0.002878424 9.52252 6.514 0.3301 0.0502 0.40251 0.003924408 9.85419 6.766 0.3416 0.0457 0.49294 0.004805697 10.07242 6.945 0.3492 0.0423 0.60462 0.005894287 10.29603 7.139 0.3570 0.0401 0.69546 0.006778614 10.45226 7.279 0.3624 0.0386 0.80272 0.007823680 10.61719 7.431 0.3681 0.0374 0.91951 0.008962605 10.77887 7.583 0.3737 0.0370 1.02788 0.010017462 10.91340 7.714 0.3784 0.0357 4.48550 0.043712000 13.16695 10.258 0.4565 0.0307 7.91398 0.077115042 14.42421 11.977 0.5001 0.0254 12.20072 0.118862359 15.52855 13.884 0.5384 0.0201 14.82851 0.144477242 16.05035 15.007 0.5565 0.0161 18.44005 0.179663247 16.64080 16.572 0.5769 0.0131 22.11385 0.215438416 17.14180 18.210 0.5943 0.0106 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Horvath-Kawazoe Cumulative Pore Volume Plot Slit Pore Geometry (Original H-K) ACF 1 Pore Width (Å) Pore Volume (cm³/g) 3.99872 0.0243684 3.86554 0.04874 3.92003 0.0731299 4.08181 0.0975104 4.26436 0.121842 4.44524 0.14618 4.62333 0.170416 4.80706 0.194508 5.0065 0.218541 5.22927 0.242197 5.48383 0.265349 5.78499 0.28833 6.15698 0.311708 6.21624 0.315182 6.51434 0.330147 6.76617 0.341646 6.94509 0.349212 7.13854 0.356965 7.27871 0.362381 7.43141 0.368099 7.58305 0.373705 7.71375 0.378369 10.2577 0.4565 11.9772 0.500089 13.884 0.538377 15.0074 0.556468 16.572 0.576939 18.2098 0.594308 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Horvath-Kawazoe Differential Pore Volume Plot Slit Pore Geometry (Original H-K) ACF 1 Pore Width (Å) dV/dw (cm³/g·Å) 3.99872 0.00609404 3.86554 -0.183002 3.92003 0.447591 4.08181 0.150708 4.26436 0.133281 4.44524 0.134558 4.62333 0.13609 4.80706 0.131124 5.0065 0.120507 5.22927 0.106188 5.48383 0.090946 5.78499 0.076308 6.15698 0.0628471 6.21624 0.058633 6.51434 0.0501985 6.76617 0.0456637 6.94509 0.0422863 7.13854 0.0400742 7.27871 0.0386442 7.43141 0.037446 7.58305 0.036967 7.71375 0.0356868 10.2577 0.0307125 11.9772 0.02535 13.884 0.0200797 15.0074 0.0161031 16.572 0.0130834 18.2098 0.0106062 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Porosity Distribution by Invalid Model: N2 @ 77 on Carbon Slit Pores by NLDFT Method: Non-negative Regularization: 0.03160 Standard Deviation of Fit: 0.297092 mmol/g Volume in Pores < 7.30 Å : 0.06761 cm³/g Total Volume in Pores <= 261.41 Å : 0.72103 cm³/g Area in Pores > 261.41 Å : 0.000 m²/g Total Area in Pores >= 7.30 Å : 803.676 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 7.30 0.10915 0.04154 113.799 113.799 7.66 0.13725 0.02810 187.178 73.379 8.01 0.14609 0.00885 209.256 22.077 8.37 0.14609 0.00000 209.256 0.000 8.73 0.14609 0.00000 209.256 0.000 9.08 0.14609 0.00000 209.256 0.000 9.62 0.14609 0.00000 209.256 0.000 9.98 0.14609 0.00000 209.256 0.000 10.51 0.14805 0.00196 212.981 3.726 10.87 0.16154 0.01349 237.809 24.828 11.40 0.18598 0.02444 280.675 42.866 11.94 0.21270 0.02672 325.437 44.762 12.47 0.24000 0.02729 369.204 43.766 13.01 0.27063 0.03063 416.298 47.095 13.54 0.29868 0.02805 457.723 41.424 14.26 0.32098 0.02230 489.007 31.284 14.79 0.33696 0.01598 510.613 21.606 15.43 0.35245 0.01549 530.684 20.071 16.29 0.37450 0.02206 557.764 27.081 16.86 0.39967 0.02516 587.612 29.848 17.72 0.42198 0.02231 612.800 25.188 18.57 0.43855 0.01657 630.648 17.847 19.43 0.45286 0.01431 645.374 14.726 20.28 0.46043 0.00758 652.844 7.471 21.14 0.46043 0.00000 652.844 0.000 22.00 0.46230 0.00187 654.540 1.696 23.14 0.47289 0.01059 663.693 9.153 23.99 0.48709 0.01420 675.529 11.836 25.14 0.50333 0.01624 688.454 12.925 26.28 0.51998 0.01665 701.122 12.669 27.42 0.53498 0.01500 712.067 10.945 28.85 0.54742 0.01244 720.691 8.623 29.99 0.56001 0.01260 729.091 8.400 31.41 0.57331 0.01329 737.555 8.464 32.84 0.58768 0.01437 746.306 8.751 34.27 0.60118 0.01350 754.187 7.881 35.98 0.61192 0.01074 760.159 5.972 37.69 0.62103 0.00911 764.992 4.834 39.12 0.62953 0.00849 769.335 4.343 41.12 0.64013 0.01060 774.492 5.156 42.83 0.65253 0.01241 780.285 5.793 44.83 0.66361 0.01108 785.226 4.942 46.82 0.66878 0.00517 787.436 2.209 48.82 0.67663 0.00785 790.650 3.214 51.10 0.68631 0.00968 794.440 3.790 53.39 0.69107 0.00476 796.222 1.781 55.95 0.69500 0.00393 797.626 1.404 58.52 0.69500 0.00000 797.626 0.000 61.09 0.69629 0.00129 798.048 0.422 63.66 0.70197 0.00568 799.833 1.785 66.80 0.70376 0.00179 800.369 0.536 69.65 0.70644 0.00268 801.139 0.771 72.79 0.70644 0.00000 801.139 0.000 76.22 0.70644 0.00000 801.139 0.000 79.64 0.70644 0.00000 801.139 0.000 83.06 0.71041 0.00397 802.095 0.956 86.77 0.71041 0.00000 802.095 0.000 90.77 0.71041 0.00000 802.095 0.000 94.76 0.71041 0.00000 802.095 0.000 99.04 0.71331 0.00290 802.681 0.586 103.61 0.71331 0.00000 802.681 0.000 108.18 0.71331 0.00000 802.681 0.000 113.03 0.71331 0.00000 802.681 0.000 118.16 0.71331 0.00000 802.681 0.000 123.59 0.71331 0.00000 802.681 0.000 129.29 0.71627 0.00296 803.139 0.458 135.00 0.71658 0.00031 803.184 0.045 140.99 0.71692 0.00035 803.233 0.049 147.27 0.71722 0.00030 803.274 0.041 154.12 0.71748 0.00025 803.307 0.033 160.97 0.71794 0.00046 803.364 0.057 168.10 0.71835 0.00041 803.413 0.049 175.81 0.71864 0.00029 803.446 0.032 183.80 0.71909 0.00045 803.495 0.049 192.07 0.71946 0.00037 803.534 0.039 200.63 0.71972 0.00026 803.559 0.026 209.76 0.72010 0.00038 803.596 0.037 219.18 0.72041 0.00031 803.624 0.029 228.88 0.72063 0.00021 803.643 0.019 239.44 0.72083 0.00020 803.660 0.017 250.00 0.72103 0.00020 803.676 0.016 261.41 0.72103 0.00000 803.676 0.000 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Porosity Distribution by Invalid Model: N2 @ 77 on Carbon Slit Pores by NLDFT Method: Non-negative Regularization: 0.03160 Standard Deviation of Fit: 0.297092 mmol/g Isotherm Table Experimental Fitted Relative Quantity Quantity Absolute Pressure Adsorbed Adsorbed Residual Relative (p/p°) (mmol/g) (mmol/g) (mmol/g) Residual ----- 0.000007523 0.89330 1.52061 -0.62730 -0.702230 0.000009404 2.56965 2.46156 0.10809 0.042064 0.000011755 2.96953 2.57097 0.39856 0.134216 0.000014694 3.21354 3.19864 0.01490 0.004638 0.000018367 3.44446 3.31191 0.13255 0.038482 0.000022959 3.64997 3.55859 0.09139 0.025038 0.000028699 3.90917 3.67006 0.23911 0.061167 0.000035873 4.18831 3.78192 0.40639 0.097030 0.000044842 4.44777 3.90189 0.54588 0.122731 0.000056052 4.73957 4.03956 0.70001 0.147695 0.000070065 5.01677 4.21159 0.80518 0.160498 0.000087581 5.31267 4.46076 0.85190 0.160353 0.000109476 5.60899 4.95739 0.65160 0.116171 0.000136846 5.89714 5.83474 0.06240 0.010581 0.000171057 6.20325 6.79816 -0.59491 -0.095902 0.000213821 6.47978 7.35002 -0.87025 -0.134302 0.000267276 6.77859 7.70605 -0.92746 -0.136822 0.000334096 7.05190 7.97873 -0.92683 -0.131430 0.000417619 7.32998 8.20354 -0.87356 -0.119177 0.000522024 7.61070 8.39674 -0.78604 -0.103281 0.000652530 7.86164 8.56740 -0.70576 -0.089772 0.000815663 8.13909 8.72126 -0.58218 -0.071529 0.001019580 8.37569 8.86241 -0.48672 -0.058111 0.001274470 8.61251 8.99416 -0.38165 -0.044313 0.001593090 8.87872 9.12857 -0.24985 -0.028141 0.001991360 9.13240 9.33563 -0.20322 -0.022253 0.002489210 9.36812 9.47194 -0.10382 -0.011082 0.003111510 9.60357 9.59083 0.01274 0.001327 0.003889380 9.84484 9.86862 -0.02379 -0.002416 0.004861730 10.08461 9.99627 0.08834 0.008760 0.006077160 10.32972 10.11249 0.21723 0.021030 0.007596450 10.58284 10.39340 0.18944 0.017900 0.009495570 10.85101 10.52577 0.32523 0.029973 0.011869500 11.10682 10.82130 0.28552 0.025707 0.014836800 11.39406 11.24789 0.14617 0.012828 0.018546000 11.71683 11.42560 0.29124 0.024856 0.023182500 12.06977 11.92779 0.14198 0.011763 0.028978200 12.44396 12.38494 0.05903 0.004743 0.036222700 12.83047 12.75016 0.08031 0.006260 0.045278400 13.23303 13.10115 0.13189 0.009966 0.056598000 13.70238 13.55771 0.14467 0.010558 0.070747500 14.22764 14.11293 0.11471 0.008062 0.088434400 14.74552 14.66526 0.08026 0.005443 0.110543000 15.33559 15.35989 -0.02430 -0.001585 0.116070000 15.46621 15.42047 0.04574 0.002957 0.121874000 15.59413 15.48871 0.10542 0.006760 0.127967000 15.72475 15.67860 0.04615 0.002935 0.134366000 15.85708 15.77738 0.07970 0.005026 0.141084000 15.98810 15.92812 0.05998 0.003752 0.148138000 16.11573 16.13191 -0.01617 -0.001004 0.155545000 16.24641 16.30192 -0.05551 -0.003417 0.163322000 16.37996 16.44380 -0.06384 -0.003897 0.171488000 16.51431 16.53895 -0.02464 -0.001492 0.180063000 16.64675 16.62170 0.02505 0.001505 0.189066000 16.77939 16.69656 0.08283 0.004936 0.198519000 16.91466 16.89592 0.01874 0.001108 0.208445000 17.05065 16.96073 0.08992 0.005274 0.218867000 17.18536 17.20672 -0.02135 -0.001243 0.229811000 17.32317 17.26580 0.05737 0.003312 0.241301000 17.46428 17.54004 -0.07576 -0.004338 0.253366000 17.60643 17.59560 0.01082 0.000615 0.266035000 17.75218 17.65032 0.10187 0.005738 0.279337000 17.90239 17.92879 -0.02640 -0.001475 0.293303000 18.05603 17.98196 0.07407 0.004102 0.307969000 18.21551 18.24694 -0.03143 -0.001725 0.323367000 18.37950 18.29950 0.08000 0.004352 0.339535000 18.54986 18.53321 0.01664 0.000897 0.356512000 18.72717 18.77300 -0.04583 -0.002447 0.374338000 18.91208 18.82624 0.08583 0.004539 0.393055000 19.10415 19.08504 0.01911 0.001000 0.412707000 19.30333 19.36538 -0.06204 -0.003214 0.433343000 19.51018 19.42242 0.08776 0.004498 0.455010000 19.72651 19.69818 0.02833 0.001436 0.477760000 19.95309 19.93844 0.01465 0.000734 0.501648000 20.18988 20.16705 0.02283 0.001131 0.526731000 20.43571 20.41828 0.01743 0.000853 0.553067000 20.68812 20.67372 0.01440 0.000696 0.580721000 20.94654 20.93603 0.01051 0.000502 0.609757000 21.20238 21.17167 0.03071 0.001448 0.640244000 21.44916 21.44095 0.00821 0.000383 0.672257000 21.67929 21.65679 0.02249 0.001038 0.705870000 21.88178 21.85832 0.02346 0.001072 0.741163000 22.05485 22.03836 0.01649 0.000748 0.778221000 22.19900 22.17701 0.02200 0.000991 0.817132000 22.31959 22.30185 0.01774 0.000795 0.857989000 22.42501 22.40723 0.01778 0.000793 0.899898000 22.52165 22.51814 0.00351 0.000156 0.903995000 22.53042 22.52879 0.00163 0.000072 0.907932000 22.53895 22.54024 -0.00129 -0.000057 0.911716000 22.54748 22.54409 0.00339 0.000150 0.915352000 22.55617 22.55428 0.00189 0.000084 0.918845000 22.56516 22.56339 0.00177 0.000078 0.922200000 22.57453 22.57694 -0.00241 -0.000107 0.925422000 22.58435 22.58029 0.00407 0.000180 0.928516000 22.59430 22.59275 0.00155 0.000069 0.931486000 22.60385 22.60240 0.00145 0.000064 0.934337000 22.61302 22.61538 -0.00237 -0.000105 0.937074000 22.62182 22.61804 0.00378 0.000167 0.939700000 22.63026 22.62896 0.00130 0.000058 0.942221000 22.63837 22.63715 0.00121 0.000054 0.944638000 22.64614 22.64820 -0.00206 -0.000091 0.946958000 22.65360 22.65038 0.00322 0.000142 0.949183000 22.66075 22.65966 0.00109 0.000048 0.951317000 22.66761 22.66661 0.00101 0.000045 0.953364000 22.67420 22.67327 0.00093 0.000041 0.955327000 22.68051 22.67975 0.00076 0.000034 0.957209000 22.68656 22.68147 0.00509 0.000224 0.959013000 22.69236 22.68312 0.00924 0.000407 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Å) Cumulative Surface Area (m²/g) 7.301 113.799 7.6577 187.178 8.0144 209.256 8.3711 209.256 8.7278 209.256 9.0845 209.256 9.6195 209.256 9.9762 209.256 10.5113 212.981 10.868 237.809 11.403 280.675 11.9381 325.437 12.4731 369.204 13.0082 416.298 13.5432 457.723 14.2566 489.007 14.7917 510.613 15.4338 530.684 16.2898 557.764 16.8606 587.612 17.7166 612.8 18.5727 630.648 19.4288 645.374 20.2849 652.844 21.141 652.844 21.997 654.54 23.1385 663.693 23.9946 675.529 25.136 688.454 26.2774 701.122 27.4189 712.067 28.8457 720.691 29.9871 729.091 31.4139 737.555 32.8407 746.306 34.2675 754.187 35.9797 760.159 37.6918 764.992 39.1186 769.335 41.1162 774.492 42.8283 780.285 44.8258 785.226 46.8234 787.436 48.8209 790.65 51.1038 794.44 53.3866 796.222 55.9549 797.626 58.5231 797.626 61.0914 798.048 63.6596 799.833 66.7986 800.369 69.6522 801.139 72.7911 801.139 76.2154 801.139 79.6398 801.139 83.0641 802.095 86.7738 802.095 90.7688 802.095 94.7638 802.095 99.0442 802.681 103.61 802.681 108.176 802.681 113.027 802.681 118.163 802.681 123.585 802.681 129.292 803.139 135 803.184 140.992 803.233 147.27 803.274 154.119 803.307 160.967 803.364 168.101 803.413 175.806 803.446 183.796 803.495 192.072 803.534 200.632 803.559 209.764 803.596 219.181 803.624 228.883 803.643 239.441 803.66 250 803.676 261.414 803.676 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Å) Incremental Surface Area (m²/g) 7.301 113.799 7.6577 73.3789 8.0144 22.0772 8.3711 0 8.7278 0 9.0845 0 9.6195 0 9.9762 0 10.5113 3.72568 10.868 24.8281 11.403 42.8659 11.9381 44.7622 12.4731 43.7661 13.0082 47.0949 13.5432 41.4243 14.2566 31.2845 14.7917 21.6055 15.4338 20.0709 16.2898 27.0805 16.8606 29.8481 17.7166 25.1882 18.5727 17.8472 19.4288 14.7262 20.2849 7.47062 21.141 0 21.997 1.69575 23.1385 9.15261 23.9946 11.8358 25.136 12.9251 26.2774 12.6689 27.4189 10.9449 28.8457 8.62317 29.9871 8.40036 31.4139 8.46413 32.8407 8.75113 34.2675 7.8807 35.9797 5.97175 37.6918 4.83375 39.1186 4.34299 41.1162 5.15643 42.8283 5.79292 44.8258 4.94162 46.8234 2.20926 48.8209 3.21449 51.1038 3.79031 53.3866 1.7814 55.9549 1.40409 58.5231 0 61.0914 0.422229 63.6596 1.78471 66.7986 0.535991 69.6522 0.770641 72.7911 0 76.2154 0 79.6398 0 83.0641 0.955678 86.7738 0 90.7688 0 94.7638 0 99.0442 0.585768 103.61 0 108.176 0 113.027 0 118.163 0 123.585 0 129.292 0.457744 135 0.0454804 140.992 0.0490271 147.27 0.0406881 154.119 0.0329065 160.967 0.0573622 168.101 0.0490518 175.806 0.0324632 183.796 0.0489742 192.072 0.0389634 200.632 0.0255553 209.764 0.0366155 219.181 0.0286061 228.883 0.0187158 239.441 0.0170577 250 0.0159633 261.414 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dA/dW Surface Area vs. Pore Width dA/dW Surface Area Pore Width (Å) dA/dW Surface Area (m²/g·Å) 7.301 319.034 7.6577 205.716 8.0144 61.893 8.3711 0 8.7278 0 9.0845 0 9.6195 0 9.9762 0 10.5113 8.35541 10.868 55.6871 11.403 80.1157 11.9381 83.6598 12.4731 81.7981 13.0082 88.0195 13.5432 66.3639 14.2566 50.1153 14.7917 36.7066 15.4338 26.7951 16.2898 37.9598 16.8606 41.8392 17.7166 29.4238 18.5727 20.8471 19.4288 17.2015 20.2849 8.72634 21.141 0 21.997 1.69788 23.1385 9.1636 23.9946 11.8506 25.136 11.3239 26.2774 11.099 27.4189 8.52309 28.8457 6.71534 29.9871 6.54183 31.4139 5.93225 32.8407 6.1334 34.2675 5.02116 35.9797 3.48787 37.6918 3.0799 39.1186 2.53649 41.1162 2.77997 42.8283 3.12321 44.8258 2.47384 46.8234 1.10598 48.8209 1.50196 51.1038 1.66034 53.3866 0.734431 55.9549 0.546711 58.5231 0 61.0914 0.164403 63.6596 0.625423 66.7986 0.178884 69.6522 0.257202 72.7911 0 76.2154 0 79.6398 0 83.0641 0.267922 86.7738 0 90.7688 0 94.7638 0 99.0442 0.132434 103.61 0 108.176 0 113.027 0 118.163 0 123.585 0 129.292 0.0802047 135 0.00777456 140.992 0.00799106 147.27 0.00619938 154.119 0.00480482 160.967 0.00820474 168.101 0.00661134 175.806 0.00413681 183.796 0.00602185 192.072 0.00462852 200.632 0.00288887 209.764 0.0039481 219.181 0.00299241 228.883 0.00184751 239.441 0.00161557 250 0.00145301 261.414 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dA/dlog(W) Surface Area vs. Pore Width dA/dlog(W) Surface Area Pore Width (Å) dA/dlog(W) Surface Area (m²/g) 7.301 5493.31 7.6577 3624.66 8.0144 1141.41 8.3711 0 8.7278 0 9.0845 0 9.6195 0 9.9762 0 10.5113 200.389 10.868 1404.2 11.403 2102.01 11.9381 2298.13 12.4731 2347.84 13.0082 2634.91 13.5432 2081.69 14.2566 1633.79 14.7917 1254.06 15.4338 958.091 16.2898 1410.44 16.8606 1637.1 17.7166 1199.38 18.5727 890.9 19.4288 769.035 20.2849 407.345 21.141 0 21.997 86.4967 23.1385 484.905 23.9946 658.258 25.136 654.949 26.2774 671.131 27.4189 540.507 28.8457 443.528 29.9871 453.574 31.4139 428.803 32.8407 463.507 34.2675 397.562 35.9797 288.738 37.6918 266.133 39.1186 229.994 41.1162 262.096 42.8283 308.832 44.8258 255.169 46.8234 119.169 48.8209 169.227 51.1038 195.244 53.3866 90.4609 55.9549 70.3892 58.5231 0 61.0914 23.1127 63.6596 92.0254 66.7986 27.4368 69.6522 41.3091 72.7911 0 76.2154 0 79.6398 0 83.0641 51.3 86.7738 0 90.7688 0 94.7638 0 99.0442 30.226 103.61 0 108.176 0 113.027 0 118.163 0 123.585 0 129.292 23.862 135 2.41775 140.992 2.59526 147.27 2.1049 154.119 1.70397 160.967 3.0418 168.101 2.56172 175.806 1.67486 183.796 2.5488 192.072 2.04723 200.632 1.33561 209.764 1.90699 219.181 1.51024 228.883 0.974865 239.441 0.890139 250 0.837315 261.414 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Å) Cumulative Pore Volume (cm³/g) 7.301 0.10915 7.6577 0.137246 8.0144 0.146092 8.3711 0.146092 8.7278 0.146092 9.0845 0.146092 9.6195 0.146092 9.9762 0.146092 10.5113 0.14805 10.868 0.161542 11.403 0.185982 11.9381 0.212701 12.4731 0.239996 13.0082 0.270627 13.5432 0.298678 14.2566 0.320978 14.7917 0.336957 15.4338 0.352446 16.2898 0.374502 16.8606 0.399665 17.7166 0.421978 18.5727 0.438551 19.4288 0.452857 20.2849 0.460434 21.141 0.460434 21.997 0.462299 23.1385 0.472888 23.9946 0.487088 25.136 0.503332 26.2774 0.519977 27.4189 0.534982 28.8457 0.547419 29.9871 0.560014 31.4139 0.573309 32.8407 0.587678 34.2675 0.601181 35.9797 0.611924 37.6918 0.621034 39.1186 0.629528 41.1162 0.640129 42.8283 0.652534 44.8258 0.66361 46.8234 0.668782 48.8209 0.676629 51.1038 0.686314 53.3866 0.691069 55.9549 0.694997 58.5231 0.694997 61.0914 0.696287 63.6596 0.701967 66.7986 0.703758 69.6522 0.706441 72.7911 0.706441 76.2154 0.706441 79.6398 0.706441 83.0641 0.710411 86.7738 0.710411 90.7688 0.710411 94.7638 0.710411 99.0442 0.713311 103.61 0.713311 108.176 0.713311 113.027 0.713311 118.163 0.713311 123.585 0.713311 129.292 0.716271 135 0.716578 140.992 0.716923 147.27 0.717223 154.119 0.717476 160.967 0.717938 168.101 0.71835 175.806 0.718636 183.796 0.719086 192.072 0.71946 200.632 0.719716 209.764 0.7201 219.181 0.720414 228.883 0.720628 239.441 0.720832 250 0.721032 261.414 0.721032 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Å) Incremental Pore Volume (cm³/g) 7.301 0.0415425 7.6577 0.0280957 8.0144 0.00884679 8.3711 0 8.7278 0 9.0845 0 9.6195 0 9.9762 0 10.5113 0.00195809 10.868 0.0134916 11.403 0.02444 11.9381 0.0267188 12.4731 0.0272949 13.0082 0.030631 13.5432 0.0280509 14.2566 0.0223005 14.7917 0.0159791 15.4338 0.0154885 16.2898 0.0220568 16.8606 0.0251628 17.7166 0.0223125 18.5727 0.0165735 19.4288 0.0143056 20.2849 0.00757704 21.141 0 21.997 0.00186507 23.1385 0.0105889 23.9946 0.0141998 25.136 0.0162442 26.2774 0.0166453 27.4189 0.0150049 28.8457 0.0124371 29.9871 0.0125951 31.4139 0.0132946 32.8407 0.0143697 34.2675 0.0135026 35.9797 0.0107431 37.6918 0.00910964 39.1186 0.00849457 41.1162 0.0106006 42.8283 0.0124051 44.8258 0.0110756 46.8234 0.00517224 48.8209 0.00784672 51.1038 0.00968496 53.3866 0.00475514 55.9549 0.00392829 58.5231 0 61.0914 0.00128973 63.6596 0.00568069 66.7986 0.00179017 69.6522 0.00268384 72.7911 0 76.2154 0 79.6398 0 83.0641 0.00396913 86.7738 0 90.7688 0 94.7638 0 99.0442 0.00290085 103.61 0 108.176 0 113.027 0 118.163 0 123.585 0 129.292 0.00295914 135 0.000306992 140.992 0.000345622 147.27 0.000299607 154.119 0.000253576 160.967 0.000461672 168.101 0.000412284 175.806 0.000285361 183.796 0.000450064 192.072 0.000374188 200.632 0.000256361 209.764 0.000384031 219.181 0.000313495 228.883 0.000214187 239.441 0.000204216 250 0.000199541 261.414 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dV/dW Pore Volume vs. Pore Width dV/dW Pore Volume Pore Width (Å) dV/dW Pore Volume (cm³/g·Å) 7.301 0.116463 7.6577 0.0787656 8.0144 0.0248018 8.3711 0 8.7278 0 9.0845 0 9.6195 0 9.9762 0 10.5113 0.00439131 10.868 0.0302604 11.403 0.0456779 11.9381 0.0499369 12.4731 0.0510138 13.0082 0.0572488 13.5432 0.044939 14.2566 0.0357237 14.7917 0.0271476 15.4338 0.0206775 16.2898 0.0309179 16.8606 0.0352717 17.7166 0.0260645 18.5727 0.0193594 19.4288 0.0167102 20.2849 0.00885065 21.141 0 21.997 0.00186741 23.1385 0.0106016 23.9946 0.0142175 25.136 0.0142318 26.2774 0.0145826 27.4189 0.0116847 28.8457 0.00968543 29.9871 0.00980852 31.4139 0.00931776 32.8407 0.0100713 34.2675 0.00860312 35.9797 0.00627462 37.6918 0.00580435 39.1186 0.0049612 41.1162 0.00571509 42.8283 0.00668808 44.8258 0.0055446 46.8234 0.00258929 48.8209 0.00366635 51.1038 0.00424249 53.3866 0.00196044 55.9549 0.00152956 58.5231 0 61.0914 0.000502182 63.6596 0.00199071 66.7986 0.000597461 69.6522 0.000895734 72.7911 0 76.2154 0 79.6398 0 83.0641 0.00111274 86.7738 0 90.7688 0 94.7638 0 99.0442 0.00065584 103.61 0 108.176 0 113.027 0 118.163 0 123.585 0 129.292 0.000518493 135 5.24781e-005 140.992 5.63338e-005 147.27 4.56491e-005 154.119 3.70256e-005 160.967 6.60348e-005 168.101 5.55688e-005 175.806 3.63638e-005 183.796 5.53397e-005 192.072 4.44504e-005 200.632 2.898e-005 209.764 4.14085e-005 219.181 3.27939e-005 228.883 2.11432e-005 239.441 1.93417e-005 250 1.81626e-005 261.414 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dV/dlog(W) Pore Volume vs. Pore Width dV/dlog(W) Pore Volume Pore Width (Å) dV/dlog(W) Pore Volume (cm³/g) 7.301 2.00533 7.6577 1.38783 8.0144 0.457385 8.3711 0 8.7278 0 9.0845 0 9.6195 0 9.9762 0 10.5113 0.105317 10.868 0.763041 11.403 1.19846 11.9381 1.37177 12.4731 1.46424 13.0082 1.71377 13.5432 1.40964 14.2566 1.16461 14.7917 0.927484 15.4338 0.739349 16.2898 1.14879 16.8606 1.38012 17.7166 1.06245 18.5727 0.827321 19.4288 0.747071 20.2849 0.413148 21.141 0 21.997 0.0951334 23.1385 0.560999 23.9946 0.789732 25.136 0.82314 26.2774 0.881779 27.4189 0.741006 28.8457 0.639694 29.9871 0.680068 31.4139 0.673519 32.8407 0.761094 34.2675 0.681173 35.9797 0.519436 37.6918 0.501552 39.1186 0.449852 41.1162 0.538821 42.8283 0.661337 44.8258 0.571909 46.8234 0.278995 48.8209 0.413091 51.1038 0.498884 53.3866 0.24147 55.9549 0.196931 58.5231 0 61.0914 0.0705993 63.6596 0.292915 66.7986 0.091637 69.6522 0.143864 72.7911 0 76.2154 0 79.6398 0 83.0641 0.213059 86.7738 0 90.7688 0 94.7638 0 99.0442 0.149686 103.61 0 108.176 0 113.027 0 118.163 0 123.585 0 129.292 0.154259 135 0.0163198 140.992 0.0182955 147.27 0.0154995 154.119 0.0131307 160.967 0.0244815 168.101 0.0215314 175.806 0.0147226 183.796 0.023423 192.072 0.0196607 200.632 0.0133984 209.764 0.0200008 219.181 0.0165508 228.883 0.0111565 239.441 0.0106568 250 0.0104664 261.414 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Goodness of Fit Standard Deviation of Fit: 0.297092 mmol/g ACF 1 : Adsorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.34981e-006 0.702863 4.30389e-006 1.40582 5.36731e-006 2.1093 1.01313e-005 2.81252 1.98585e-005 3.51431 3.67919e-005 4.21632 6.44276e-005 4.91536 0.000109592 5.61026 0.000185348 6.30345 0.000315239 6.98576 0.000542904 7.65352 0.000957593 8.31637 0.00174926 8.99069 0.00190952 9.09089 0.00287842 9.52252 0.00392441 9.85419 0.0048057 10.0724 0.00589429 10.296 0.00677861 10.4523 0.00782368 10.6172 0.0089626 10.7789 0.0100175 10.9134 0.043712 13.1669 0.077115 14.4242 0.118862 15.5285 0.144477 16.0504 0.179663 16.6408 0.215438 17.1418 0.251251 17.582 0.284318 17.9575 0.317051 18.3126 0.34942 18.6533 0.380226 18.9727 0.413838 19.3147 0.447562 19.6522 0.481515 19.9905 0.515462 20.3259 0.549543 20.6545 0.583503 20.9721 0.617802 21.27 0.651982 21.5373 0.686311 21.7688 0.720675 21.9585 0.754872 22.1123 0.789286 22.2357 0.823486 22.337 0.857677 22.4243 0.891765 22.5036 0.925734 22.5854 0.959198 22.693 ACF 1 : model fit Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.52316e-006 1.52061 9.40395e-006 2.46156 1.17549e-005 2.57097 1.46937e-005 3.19864 1.83671e-005 3.31191 2.29589e-005 3.55859 2.86986e-005 3.67006 3.58732e-005 3.78192 4.48416e-005 3.90189 5.60519e-005 4.03956 7.00649e-005 4.21159 8.75812e-005 4.46076 0.000109476 4.95739 0.000136846 5.83474 0.000171057 6.79816 0.000213821 7.35002 0.000267276 7.70605 0.000334096 7.97873 0.000417619 8.20354 0.000522024 8.39674 0.00065253 8.5674 0.000815663 8.72126 0.00101958 8.86241 0.00127447 8.99416 0.00159309 9.12857 0.00199136 9.33563 0.00248921 9.47194 0.00311151 9.59083 0.00388938 9.86862 0.00486173 9.99627 0.00607716 10.1125 0.00759645 10.3934 0.00949557 10.5258 0.0118695 10.8213 0.0148368 11.2479 0.018546 11.4256 0.0231825 11.9278 0.0289782 12.3849 0.0362227 12.7502 0.0452784 13.1011 0.056598 13.5577 0.0707475 14.1129 0.0884344 14.6653 0.110543 15.3599 0.11607 15.4205 0.121874 15.4887 0.127967 15.6786 0.134366 15.7774 0.141084 15.9281 0.148138 16.1319 0.155545 16.3019 0.163322 16.4438 0.171488 16.5389 0.180063 16.6217 0.189066 16.6966 0.198519 16.8959 0.208445 16.9607 0.218867 17.2067 0.229811 17.2658 0.241301 17.54 0.253366 17.5956 0.266035 17.6503 0.279337 17.9288 0.293303 17.982 0.307969 18.2469 0.323367 18.2995 0.339535 18.5332 0.356512 18.773 0.374338 18.8262 0.393055 19.085 0.412707 19.3654 0.433343 19.4224 0.45501 19.6982 0.47776 19.9384 0.501648 20.1671 0.526731 20.4183 0.553067 20.6737 0.580721 20.936 0.609757 21.1717 0.640244 21.441 0.672257 21.6568 0.70587 21.8583 0.741163 22.0384 0.778221 22.177 0.817132 22.3018 0.857989 22.4072 0.899898 22.5181 0.903995 22.5288 0.907932 22.5402 0.911716 22.5441 0.915352 22.5543 0.918845 22.5634 0.9222 22.5769 0.925422 22.5803 0.928516 22.5927 0.931486 22.6024 0.934337 22.6154 0.937074 22.618 0.9397 22.629 0.942221 22.6372 0.944638 22.6482 0.946958 22.6504 0.949183 22.6597 0.951317 22.6666 0.953364 22.6733 0.955327 22.6797 0.957209 22.6815 0.959013 22.6831 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Goodness of Fit Standard Deviation of Fit: 0.297092 mmol/g ACF 1 : Adsorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.34981e-006 0.702863 4.30389e-006 1.40582 5.36731e-006 2.1093 1.01313e-005 2.81252 1.98585e-005 3.51431 3.67919e-005 4.21632 6.44276e-005 4.91536 0.000109592 5.61026 0.000185348 6.30345 0.000315239 6.98576 0.000542904 7.65352 0.000957593 8.31637 0.00174926 8.99069 0.00190952 9.09089 0.00287842 9.52252 0.00392441 9.85419 0.0048057 10.0724 0.00589429 10.296 0.00677861 10.4523 0.00782368 10.6172 0.0089626 10.7789 0.0100175 10.9134 0.043712 13.1669 0.077115 14.4242 0.118862 15.5285 0.144477 16.0504 0.179663 16.6408 0.215438 17.1418 0.251251 17.582 0.284318 17.9575 0.317051 18.3126 0.34942 18.6533 0.380226 18.9727 0.413838 19.3147 0.447562 19.6522 0.481515 19.9905 0.515462 20.3259 0.549543 20.6545 0.583503 20.9721 0.617802 21.27 0.651982 21.5373 0.686311 21.7688 0.720675 21.9585 0.754872 22.1123 0.789286 22.2357 0.823486 22.337 0.857677 22.4243 0.891765 22.5036 0.925734 22.5854 0.959198 22.693 ACF 1 : model fit Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.52316e-006 1.52061 9.40395e-006 2.46156 1.17549e-005 2.57097 1.46937e-005 3.19864 1.83671e-005 3.31191 2.29589e-005 3.55859 2.86986e-005 3.67006 3.58732e-005 3.78192 4.48416e-005 3.90189 5.60519e-005 4.03956 7.00649e-005 4.21159 8.75812e-005 4.46076 0.000109476 4.95739 0.000136846 5.83474 0.000171057 6.79816 0.000213821 7.35002 0.000267276 7.70605 0.000334096 7.97873 0.000417619 8.20354 0.000522024 8.39674 0.00065253 8.5674 0.000815663 8.72126 0.00101958 8.86241 0.00127447 8.99416 0.00159309 9.12857 0.00199136 9.33563 0.00248921 9.47194 0.00311151 9.59083 0.00388938 9.86862 0.00486173 9.99627 0.00607716 10.1125 0.00759645 10.3934 0.00949557 10.5258 0.0118695 10.8213 0.0148368 11.2479 0.018546 11.4256 0.0231825 11.9278 0.0289782 12.3849 0.0362227 12.7502 0.0452784 13.1011 0.056598 13.5577 0.0707475 14.1129 0.0884344 14.6653 0.110543 15.3599 0.11607 15.4205 0.121874 15.4887 0.127967 15.6786 0.134366 15.7774 0.141084 15.9281 0.148138 16.1319 0.155545 16.3019 0.163322 16.4438 0.171488 16.5389 0.180063 16.6217 0.189066 16.6966 0.198519 16.8959 0.208445 16.9607 0.218867 17.2067 0.229811 17.2658 0.241301 17.54 0.253366 17.5956 0.266035 17.6503 0.279337 17.9288 0.293303 17.982 0.307969 18.2469 0.323367 18.2995 0.339535 18.5332 0.356512 18.773 0.374338 18.8262 0.393055 19.085 0.412707 19.3654 0.433343 19.4224 0.45501 19.6982 0.47776 19.9384 0.501648 20.1671 0.526731 20.4183 0.553067 20.6737 0.580721 20.936 0.609757 21.1717 0.640244 21.441 0.672257 21.6568 0.70587 21.8583 0.741163 22.0384 0.778221 22.177 0.817132 22.3018 0.857989 22.4072 0.899898 22.5181 0.903995 22.5288 0.907932 22.5402 0.911716 22.5441 0.915352 22.5543 0.918845 22.5634 0.9222 22.5769 0.925422 22.5803 0.928516 22.5927 0.931486 22.6024 0.934337 22.6154 0.937074 22.618 0.9397 22.629 0.942221 22.6372 0.944638 22.6482 0.946958 22.6504 0.949183 22.6597 0.951317 22.6666 0.953364 22.6733 0.955327 22.6797 0.957209 22.6815 0.959013 22.6831 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Porosity Distribution by Invalid Model: N2 - DFT Model Method: Non-negative Regularization: 0.03160 Standard Deviation of Fit: 0.088200 mmol/g Volume in Pores < 5.00 Å : 0.00000 cm³/g Total Volume in Pores <= 100.61 Å : 0.60196 cm³/g Area in Pores > 100.61 Å : 53.443 m²/g Total Area in Pores >= 5.00 Å : 945.076 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 5.00 0.00191 0.00191 7.619 7.619 5.36 0.00877 0.00687 33.235 25.616 5.90 0.02385 0.01508 84.378 51.143 6.43 0.04872 0.02487 161.682 77.304 6.79 0.08121 0.03249 257.373 95.691 7.33 0.11714 0.03593 355.440 98.067 8.04 0.14790 0.03077 431.951 76.512 8.58 0.16133 0.01342 463.246 31.295 9.29 0.16133 0.00000 463.246 0.000 10.01 0.16133 0.00000 463.246 0.000 10.90 0.17270 0.01137 484.110 20.864 11.79 0.19983 0.02713 530.109 46.000 12.69 0.22809 0.02826 574.659 44.550 13.58 0.25127 0.02318 608.795 34.136 14.83 0.27752 0.02625 644.192 35.398 15.91 0.30288 0.02536 676.077 31.885 17.16 0.32218 0.01930 698.574 22.497 18.59 0.34337 0.02119 721.380 22.806 20.02 0.36657 0.02320 744.561 23.181 21.62 0.39139 0.02482 767.515 22.955 23.41 0.41275 0.02136 785.760 18.245 25.20 0.43271 0.01997 801.610 15.850 27.34 0.45378 0.02106 817.016 15.406 29.49 0.47094 0.01717 828.659 11.643 31.81 0.48703 0.01609 838.776 10.117 34.31 0.50521 0.01818 849.372 10.596 36.99 0.52039 0.01518 857.577 8.205 40.03 0.53532 0.01493 865.037 7.460 43.25 0.55051 0.01519 872.062 7.025 46.64 0.56484 0.01433 878.208 6.146 50.40 0.57774 0.01290 883.326 5.118 54.33 0.58787 0.01013 887.055 3.729 58.80 0.59535 0.00748 889.599 2.544 63.44 0.59979 0.00445 891.000 1.401 68.45 0.60196 0.00216 891.633 0.633 73.99 0.60196 0.00000 891.633 0.000 79.88 0.60196 0.00000 891.633 0.000 86.32 0.60196 0.00000 891.633 0.000 93.11 0.60196 0.00000 891.633 0.000 100.61 0.60196 0.00000 891.633 0.000 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Porosity Distribution by Invalid Model: N2 - DFT Model Method: Non-negative Regularization: 0.03160 Standard Deviation of Fit: 0.088200 mmol/g Isotherm Table Experimental Fitted Relative Quantity Quantity Absolute Pressure Adsorbed Adsorbed Residual Relative (p/p°) (mmol/g) (mmol/g) (mmol/g) Residual ----- 0.000008995 2.30578 2.64331 -0.33753 -0.146384 0.000015520 3.27271 3.03206 0.24066 0.073535 0.000026102 3.79267 3.77855 0.01412 0.003722 0.000042841 4.39128 4.28369 0.10759 0.024501 0.000068697 4.99235 4.78981 0.20254 0.040570 0.000107744 5.58963 5.41787 0.17176 0.030729 0.000165451 6.15889 6.14227 0.01662 0.002698 0.000249000 6.68279 6.80600 -0.12321 -0.018438 0.000367617 7.16713 7.34536 -0.17823 -0.024868 0.000532902 7.63366 7.78351 -0.14984 -0.019629 0.000759152 8.04972 8.15650 -0.10678 -0.013265 0.001063641 8.41756 8.53752 -0.11996 -0.014251 0.001466847 8.77849 8.82875 -0.05026 -0.005725 0.001992604 9.13303 9.09608 0.03695 0.004046 0.002668156 9.44311 9.44457 -0.00146 -0.000155 0.003524104 9.73861 9.69622 0.04239 0.004353 0.004594232 10.02437 9.91194 0.11242 0.011215 0.005915212 10.29991 10.27434 0.02557 0.002482 0.007526182 10.57201 10.50731 0.06470 0.006120 0.009468212 10.84745 10.94428 -0.09683 -0.008926 0.011783670 11.09811 11.13020 -0.03209 -0.002892 0.014515520 11.36425 11.30242 0.06183 0.005440 0.017706521 11.64711 11.77019 -0.12308 -0.010567 0.021398440 11.94014 11.93770 0.00244 0.000205 0.025631230 12.23613 12.10385 0.13228 0.010811 0.030442240 12.52848 12.55949 -0.03100 -0.002475 0.035865448 12.81309 12.73000 0.08309 0.006485 0.041930798 13.09089 13.15762 -0.06674 -0.005098 0.048663601 13.37547 13.33513 0.04034 0.003016 0.056084011 13.68167 13.79239 -0.11072 -0.008092 0.064206667 13.99729 13.98341 0.01388 0.000992 0.073040441 14.30192 14.18132 0.12060 0.008433 0.082588248 14.57982 14.68284 -0.10302 -0.007066 0.092847057 14.86914 14.87597 -0.00682 -0.000459 0.103808001 15.16533 15.06118 0.10416 0.006868 0.115456402 15.45217 15.55862 -0.10645 -0.006889 0.127772301 15.72063 15.71522 0.00541 0.000344 0.140730694 15.98145 15.86074 0.12072 0.007554 0.154301897 16.22468 16.28303 -0.05835 -0.003596 0.168452203 16.46519 16.40761 0.05758 0.003497 0.183144197 16.69248 16.80343 -0.11095 -0.006646 0.198337302 16.91211 16.91300 -0.00089 -0.000053 0.213988706 17.12326 17.01778 0.10547 0.006160 0.230053306 17.32619 17.42514 -0.09896 -0.005711 0.246484801 17.52621 17.52114 0.00506 0.000289 0.263235897 17.72014 17.61498 0.10516 0.005934 0.280259013 17.91264 17.96272 -0.05008 -0.002796 0.297506303 18.10197 18.05218 0.04979 0.002751 0.314930797 18.29010 18.38942 -0.09932 -0.005430 0.332486212 18.47575 18.47658 -0.00083 -0.000045 0.350127310 18.66064 18.56445 0.09619 0.005155 0.367810607 18.84456 18.93773 -0.09317 -0.004944 0.385494202 19.02679 19.02327 0.00352 0.000185 0.403138310 19.20674 19.10868 0.09806 0.005105 0.420704991 19.38360 19.43272 -0.04912 -0.002534 0.438158900 19.55833 19.51185 0.04648 0.002377 0.455466807 19.73106 19.83074 -0.09968 -0.005052 0.472598106 19.90172 19.90148 0.00024 0.000012 0.489524394 20.06999 19.96930 0.10069 0.005017 0.506219923 20.23496 20.28546 -0.05050 -0.002496 0.522661209 20.39626 20.34567 0.05059 0.002480 0.538827300 20.55201 20.64770 -0.09569 -0.004656 0.554699600 20.70364 20.70214 0.00149 0.000072 0.570261598 20.84978 20.75529 0.09448 0.004532 0.585499227 20.99038 21.03159 -0.04122 -0.001964 0.600400090 21.12242 21.08139 0.04103 0.001942 0.614954293 21.24613 21.31158 -0.06545 -0.003081 0.629153311 21.36256 21.35960 0.00296 0.000139 0.642990828 21.47008 21.40777 0.06232 0.002902 0.656461716 21.56999 21.59206 -0.02208 -0.001023 0.669562697 21.66129 21.63965 0.02165 0.000999 0.682291925 21.74397 21.76985 -0.02588 -0.001190 0.694648683 21.81862 21.81658 0.00203 0.000093 0.706633508 21.88592 21.86269 0.02324 0.001062 0.718248010 21.94645 21.94854 -0.00210 -0.000096 0.729494929 22.00124 21.99213 0.00911 0.000414 0.740377605 22.05137 22.03442 0.01694 0.000768 0.750900388 22.09634 22.07547 0.02087 0.000945 0.761068285 22.13649 22.11542 0.02106 0.000952 0.770887017 22.17375 22.15449 0.01925 0.000868 0.780362606 22.20730 22.19293 0.01437 0.000647 0.789501607 22.23629 22.23100 0.00529 0.000238 0.798311174 22.26239 22.26899 -0.00660 -0.000297 0.806798697 22.28753 22.30717 -0.01964 -0.000881 0.814971626 22.31175 22.34579 -0.03404 -0.001526 0.822837889 22.33505 22.38503 -0.04998 -0.002238 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Å) Cumulative Surface Area (m²/g) 5.00387 7.6192 5.36129 33.2347 5.89742 84.3781 6.43354 161.682 6.79096 257.373 7.32709 355.44 8.04193 431.951 8.57806 463.246 9.2929 463.246 10.0077 463.246 10.9013 484.11 11.7948 530.109 12.6884 574.659 13.5819 608.795 14.8329 644.192 15.9052 676.077 17.1561 698.574 18.5858 721.38 20.0155 744.561 21.6239 767.515 23.411 785.76 25.198 801.61 27.3426 817.016 29.4871 828.659 31.8103 838.776 34.3122 849.372 36.9929 857.577 40.0309 865.037 43.2477 872.062 46.6432 878.208 50.3961 883.326 54.3277 887.055 58.7954 889.599 63.4419 891 68.4458 891.633 73.9858 891.633 79.8832 891.633 86.3167 891.633 93.1077 891.633 100.613 891.633 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Å) Incremental Surface Area (m²/g) 5.00387 7.6192 5.36129 25.6155 5.89742 51.1434 6.43354 77.3036 6.79096 95.691 7.32709 98.0672 8.04193 76.5116 8.57806 31.2946 9.2929 0 10.0077 0 10.9013 20.8635 11.7948 45.9996 12.6884 44.5498 13.5819 34.1358 14.8329 35.3976 15.9052 31.8847 17.1561 22.497 18.5858 22.8061 20.0155 23.1806 21.6239 22.9546 23.411 18.2448 25.198 15.8501 27.3426 15.4059 29.4871 11.6429 31.8103 10.1165 34.3122 10.5961 36.9929 8.20514 40.0309 7.46009 43.2477 7.0253 46.6432 6.14609 50.3961 5.11771 54.3277 3.7287 58.7954 2.54429 63.4419 1.4013 68.4458 0.63252 73.9858 0 79.8832 0 86.3167 0 93.1077 0 100.613 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dA/dW Surface Area vs. Pore Width dA/dW Surface Area Pore Width (Å) dA/dW Surface Area (m²/g·Å) 5.00387 21.3173 5.36129 57.3344 5.89742 95.3938 6.43354 173.026 6.79096 214.182 7.32709 156.786 8.04193 122.324 8.57806 50.0327 9.2929 0 10.0077 0 10.9013 23.3491 11.7948 51.4798 12.6884 49.8572 13.5819 31.8354 14.8329 30.4728 15.9052 27.4487 17.1561 16.7848 18.5858 15.9519 20.0155 15.2601 21.6239 13.5207 23.411 10.2092 25.198 8.06292 27.3426 7.18385 29.4871 5.21198 31.8103 4.19324 34.3122 4.0891 36.9929 2.86958 40.0309 2.38538 43.2477 2.12493 46.6432 1.71958 50.3961 1.33195 54.3277 0.887855 58.7954 0.558314 63.4419 0.290414 68.4458 0.119979 73.9858 0 79.8832 0 86.3167 0 93.1077 0 100.613 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dA/dlog(W) Surface Area vs. Pore Width dA/dlog(W) Surface Area Pore Width (Å) dA/dlog(W) Surface Area (m²/g) 5.00387 254.285 5.36129 717.965 5.89742 1291.8 6.43354 2523.39 6.79096 3388.41 7.32709 2671.08 8.04193 2235.3 8.57806 996.789 9.2929 0 10.0077 0 10.9013 584.773 11.7948 1395.44 12.6884 1454.22 13.5819 1006.66 14.8329 1032.36 15.9052 1009.12 17.1561 665.166 18.5858 681.32 20.0155 705.091 21.6239 674.607 23.411 549.262 25.198 470.19 27.3426 451.356 29.4871 354.271 31.8103 307.413 34.3122 323.295 36.9929 245.124 40.0309 219.916 43.2477 211.629 46.6432 185.029 50.3961 154.536 54.3277 111.393 58.7954 75.549 63.4419 42.4617 68.4458 18.9457 73.9858 0 79.8832 0 86.3167 0 93.1077 0 100.613 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Å) Cumulative Pore Volume (cm³/g) 5.00387 0.00190627 5.36129 0.00877287 5.89742 0.0238536 6.43354 0.0487204 6.79096 0.0812121 7.32709 0.117139 8.04193 0.147904 8.57806 0.161327 9.2929 0.161327 10.0077 0.161327 10.9013 0.172699 11.7948 0.199827 12.6884 0.22809 13.5819 0.251271 14.8329 0.277524 15.9052 0.30288 17.1561 0.322178 18.5858 0.343372 20.0155 0.36657 21.6239 0.391389 23.411 0.412745 25.198 0.432715 27.3426 0.453777 29.4871 0.470942 31.8103 0.487033 34.3122 0.505211 36.9929 0.520388 40.0309 0.53532 43.2477 0.550511 46.6432 0.564845 50.3961 0.57774 54.3277 0.587869 58.7954 0.595349 63.4419 0.599794 68.4458 0.601958 73.9858 0.601958 79.8832 0.601958 86.3167 0.601958 93.1077 0.601958 100.613 0.601958 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Å) Incremental Pore Volume (cm³/g) 5.00387 0.00190627 5.36129 0.0068666 5.89742 0.0150807 6.43354 0.0248668 6.79096 0.0324917 7.32709 0.0359274 8.04193 0.030765 8.57806 0.0134223 9.2929 0 10.0077 0 10.9013 0.011372 11.7948 0.0271279 12.6884 0.0282632 13.5819 0.0231815 14.8329 0.0262525 15.9052 0.0253565 17.1561 0.0192981 18.5858 0.0211935 20.0155 0.0231985 21.6239 0.0248184 23.411 0.0213564 25.198 0.0199696 27.3426 0.0210618 29.4871 0.0171657 31.8103 0.0160905 34.3122 0.0181787 36.9929 0.0151766 40.0309 0.0149317 43.2477 0.0151914 46.6432 0.0143337 50.3961 0.0128956 54.3277 0.0101286 58.7954 0.00747964 63.4419 0.00444504 68.4458 0.00216466 73.9858 0 79.8832 0 86.3167 0 93.1077 0 100.613 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dV/dW Pore Volume vs. Pore Width dV/dW Pore Volume Pore Width (Å) dV/dW Pore Volume (cm³/g·Å) 5.00387 0.00533344 5.36129 0.0153693 5.89742 0.0281288 6.43354 0.0556586 6.79096 0.0727252 7.32709 0.0574394 8.04193 0.049186 8.57806 0.0214592 9.2929 0 10.0077 0 10.9013 0.0127267 11.7948 0.0303597 12.6884 0.0316304 13.5819 0.0216193 14.8329 0.0226 15.9052 0.0218287 17.1561 0.0143981 18.5858 0.014824 20.0155 0.0152719 21.6239 0.0146185 23.411 0.0119503 25.198 0.0101585 27.3426 0.00982124 29.4871 0.0076843 31.8103 0.00666942 34.3122 0.00701531 36.9929 0.0053077 40.0309 0.00477446 43.2477 0.00459493 46.6432 0.00401033 50.3961 0.00335626 54.3277 0.00241176 58.7954 0.00164132 63.4419 0.000921222 68.4458 0.000410602 73.9858 0 79.8832 0 86.3167 0 93.1077 0 100.613 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No dV/dlog(W) Pore Volume vs. Pore Width dV/dlog(W) Pore Volume Pore Width (Å) dV/dlog(W) Pore Volume (cm³/g) 5.00387 0.0636204 5.36129 0.192461 5.89742 0.380915 6.43354 0.811717 6.79096 1.15053 7.32709 0.978562 8.04193 0.898808 8.57806 0.427526 9.2929 0 10.0077 0 10.9013 0.318739 11.7948 0.822948 12.6884 0.922586 13.5819 0.683621 14.8329 0.765641 15.9052 0.802509 17.1561 0.570583 18.5858 0.633143 20.0155 0.705636 21.6239 0.72938 23.411 0.642937 25.198 0.592393 27.3426 0.617061 29.4871 0.522321 31.8103 0.488945 34.3122 0.554649 36.9929 0.453393 40.0309 0.440171 43.2477 0.457624 46.6432 0.431518 50.3961 0.389401 54.3277 0.302586 58.7954 0.222097 63.4419 0.134692 68.4458 0.0648375 73.9858 0 79.8832 0 86.3167 0 93.1077 0 100.613 0 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Goodness of Fit Standard Deviation of Fit: 0.088200 mmol/g ACF 1 : Adsorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.34981e-006 0.702863 4.30389e-006 1.40582 5.36731e-006 2.1093 1.01313e-005 2.81252 1.98585e-005 3.51431 3.67919e-005 4.21632 6.44276e-005 4.91536 0.000109592 5.61026 0.000185348 6.30345 0.000315239 6.98576 0.000542904 7.65352 0.000957593 8.31637 0.00174926 8.99069 0.00190952 9.09089 0.00287842 9.52252 0.00392441 9.85419 0.0048057 10.0724 0.00589429 10.296 0.00677861 10.4523 0.00782368 10.6172 0.0089626 10.7789 0.0100175 10.9134 0.043712 13.1669 0.077115 14.4242 0.118862 15.5285 0.144477 16.0504 0.179663 16.6408 0.215438 17.1418 0.251251 17.582 0.284318 17.9575 0.317051 18.3126 0.34942 18.6533 0.380226 18.9727 0.413838 19.3147 0.447562 19.6522 0.481515 19.9905 0.515462 20.3259 0.549543 20.6545 0.583503 20.9721 0.617802 21.27 0.651982 21.5373 0.686311 21.7688 0.720675 21.9585 0.754872 22.1123 0.789286 22.2357 0.823486 22.337 ACF 1 : model fit Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 8.99464e-006 2.64331 1.552e-005 3.03206 2.61021e-005 3.77855 4.28409e-005 4.28369 6.86973e-005 4.78981 0.000107744 5.41787 0.000165451 6.14227 0.000249 6.806 0.000367617 7.34536 0.000532902 7.78351 0.000759152 8.1565 0.00106364 8.53752 0.00146685 8.82875 0.0019926 9.09608 0.00266816 9.44457 0.0035241 9.69622 0.00459423 9.91194 0.00591521 10.2743 0.00752618 10.5073 0.00946821 10.9443 0.0117837 11.1302 0.0145155 11.3024 0.0177065 11.7702 0.0213984 11.9377 0.0256312 12.1038 0.0304422 12.5595 0.0358654 12.73 0.0419308 13.1576 0.0486636 13.3351 0.056084 13.7924 0.0642067 13.9834 0.0730404 14.1813 0.0825882 14.6828 0.0928471 14.876 0.103808 15.0612 0.115456 15.5586 0.127772 15.7152 0.140731 15.8607 0.154302 16.283 0.168452 16.4076 0.183144 16.8034 0.198337 16.913 0.213989 17.0178 0.230053 17.4251 0.246485 17.5211 0.263236 17.615 0.280259 17.9627 0.297506 18.0522 0.314931 18.3894 0.332486 18.4766 0.350127 18.5644 0.367811 18.9377 0.385494 19.0233 0.403138 19.1087 0.420705 19.4327 0.438159 19.5118 0.455467 19.8307 0.472598 19.9015 0.489524 19.9693 0.50622 20.2855 0.522661 20.3457 0.538827 20.6477 0.5547 20.7021 0.570262 20.7553 0.585499 21.0316 0.6004 21.0814 0.614954 21.3116 0.629153 21.3596 0.642991 21.4078 0.656462 21.5921 0.669563 21.6396 0.682292 21.7698 0.694649 21.8166 0.706634 21.8627 0.718248 21.9485 0.729495 21.9921 0.740378 22.0344 0.7509 22.0755 0.761068 22.1154 0.770887 22.1545 0.780363 22.1929 0.789502 22.231 0.798311 22.269 0.806799 22.3072 0.814972 22.3458 0.822838 22.385 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No Goodness of Fit Standard Deviation of Fit: 0.088200 mmol/g ACF 1 : Adsorption Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 7.34981e-006 0.702863 4.30389e-006 1.40582 5.36731e-006 2.1093 1.01313e-005 2.81252 1.98585e-005 3.51431 3.67919e-005 4.21632 6.44276e-005 4.91536 0.000109592 5.61026 0.000185348 6.30345 0.000315239 6.98576 0.000542904 7.65352 0.000957593 8.31637 0.00174926 8.99069 0.00190952 9.09089 0.00287842 9.52252 0.00392441 9.85419 0.0048057 10.0724 0.00589429 10.296 0.00677861 10.4523 0.00782368 10.6172 0.0089626 10.7789 0.0100175 10.9134 0.043712 13.1669 0.077115 14.4242 0.118862 15.5285 0.144477 16.0504 0.179663 16.6408 0.215438 17.1418 0.251251 17.582 0.284318 17.9575 0.317051 18.3126 0.34942 18.6533 0.380226 18.9727 0.413838 19.3147 0.447562 19.6522 0.481515 19.9905 0.515462 20.3259 0.549543 20.6545 0.583503 20.9721 0.617802 21.27 0.651982 21.5373 0.686311 21.7688 0.720675 21.9585 0.754872 22.1123 0.789286 22.2357 0.823486 22.337 ACF 1 : model fit Relative Pressure (p/p°) Quantity Adsorbed (mmol/g) 8.99464e-006 2.64331 1.552e-005 3.03206 2.61021e-005 3.77855 4.28409e-005 4.28369 6.86973e-005 4.78981 0.000107744 5.41787 0.000165451 6.14227 0.000249 6.806 0.000367617 7.34536 0.000532902 7.78351 0.000759152 8.1565 0.00106364 8.53752 0.00146685 8.82875 0.0019926 9.09608 0.00266816 9.44457 0.0035241 9.69622 0.00459423 9.91194 0.00591521 10.2743 0.00752618 10.5073 0.00946821 10.9443 0.0117837 11.1302 0.0145155 11.3024 0.0177065 11.7702 0.0213984 11.9377 0.0256312 12.1038 0.0304422 12.5595 0.0358654 12.73 0.0419308 13.1576 0.0486636 13.3351 0.056084 13.7924 0.0642067 13.9834 0.0730404 14.1813 0.0825882 14.6828 0.0928471 14.876 0.103808 15.0612 0.115456 15.5586 0.127772 15.7152 0.140731 15.8607 0.154302 16.283 0.168452 16.4076 0.183144 16.8034 0.198337 16.913 0.213989 17.0178 0.230053 17.4251 0.246485 17.5211 0.263236 17.615 0.280259 17.9627 0.297506 18.0522 0.314931 18.3894 0.332486 18.4766 0.350127 18.5644 0.367811 18.9377 0.385494 19.0233 0.403138 19.1087 0.420705 19.4327 0.438159 19.5118 0.455467 19.8307 0.472598 19.9015 0.489524 19.9693 0.50622 20.2855 0.522661 20.3457 0.538827 20.6477 0.5547 20.7021 0.570262 20.7553 0.585499 21.0316 0.6004 21.0814 0.614954 21.3116 0.629153 21.3596 0.642991 21.4078 0.656462 21.5921 0.669563 21.6396 0.682292 21.7698 0.694649 21.8166 0.706634 21.8627 0.718248 21.9485 0.729495 21.9921 0.740378 22.0344 0.7509 22.0755 0.761068 22.1154 0.770887 22.1545 0.780363 22.1929 0.789502 22.231 0.798311 22.269 0.806799 22.3072 0.814972 22.3458 0.822838 22.385 MicroActive for ASAP 2460 2.01 MicroActive for ASAP 2460 Version 2.01 Page 1 Serial # 279 Unit 1 Port 1 Sample: ACF 1 Operator: Gio Submitter: File: F:\ASAP2460\国重 ASAP2460 原始数据备份\20180407 ACF1.SMP Started: 2018/4/7 21:47:26 Analysis Adsorptive: N2 Completed: 2018/4/8 9:17:53 Analysis Bath Temp.: 77.300 K Report Time: 2018/9/25 15:53:10 Thermal Correction: No Sample Mass: 0.0846 g Warm Free Space: 17.3026 cm³ Measured Cold Free Space: 50.9600 cm³ Equilibration Interval: 5 s Low Pressure Dose: 0.26769 mmol/g Sample Density: 1.000 g/cm³ Automatic Degas: No MP Tabular Report t = [ 13.99 / ( 0.034 - log(p/p°) ) ] ^ 0.5 Total Pore Surface Area: 1442.4523 m²/g Density Conversion Factor: 0.0015468 Average Incremental Cumulative Differential Pore Pore Pore Pore Incremental Pore Hydraulic Hydraulic Volume Volume Volume Pore Area Radius Interval (Å) Radius (Å) (cm³/g) (cm³/g) (cm³/g·Å) (m²/g) ------ 0.000 - 2.623 1.3115 0.0000 0.0000 0.0000 0.0000 2.623 - 2.800 2.7115 -0.0043 -0.0043 -0.0244 -15.9202 2.800 - 3.000 2.9000 0.0087 0.0043 0.0433 29.8628 3.000 - 3.200 3.1000 0.0066 0.0109 0.0328 21.1893 3.200 - 3.400 3.3000 0.0168 0.0277 0.0840 50.9032 3.400 - 3.600 3.5000 0.0295 0.0573 0.1477 84.4263 3.600 - 3.800 3.7000 0.0485 0.1058 0.2426 131.1511 3.800 - 4.000 3.9000 0.0518 0.1576 0.2589 132.7807 4.000 - 4.200 4.1000 0.0531 0.2107 0.2655 129.4916 4.200 - 4.400 4.3000 0.0456 0.2563 0.2280 106.0490 4.400 - 4.600 4.5000 0.0374 0.2937 0.1870 83.1118 4.600 - 4.800 4.7000 0.0260 0.3196 0.1298 55.2374 4.800 - 5.000 4.9000 0.0190 0.3386 0.0950 38.7635 5.000 - 5.200 5.1000 0.0157 0.3543 0.0785 30.7733 5.200 - 5.400 5.3000 0.0133 0.3676 0.0666 25.1387 5.400 - 5.600 5.5000 0.0124 0.3800 0.0620 22.5377 5.600 - 5.800 5.7000 0.0148 0.3948 0.0739 25.9281 5.800 - 6.000 5.9000 0.0143 0.4091 0.0715 24.2498 6.000 - 6.200 6.1000 0.0126 0.4217 0.0629 20.6199 6.200 - 6.400 6.3000 0.0121 0.4338 0.0606 19.2226 6.400 - 6.600 6.5000 0.0147 0.4485 0.0733 22.5586 6.600 - 6.800 6.7000 0.0170 0.4655 0.0852 25.4225 6.800 - 7.000 6.9000 0.0155 0.4810 0.0777 22.5123 7.000 - 7.200 7.1000 0.0179 0.4989 0.0893 25.1689 7.200 - 7.400 7.3000 0.0206 0.5196 0.1032 28.2837 7.400 - 7.600 7.5000 0.0223 0.5419 0.1117 29.7758 7.600 - 7.800 7.7000 0.0204 0.5623 0.1020 26.4815 7.800 - 8.000 7.9000 0.0214 0.5837 0.1069 27.0700 8.000 - 8.200 8.1000 0.0196 0.6032 0.0978 24.1515 8.200 - 8.400 8.3000 0.0207 0.6239 0.1034 24.9230 8.400 - 8.600 8.5000 0.0192 0.6431 0.0958 22.5466 8.600 - 8.800 8.7000 0.0150 0.6581 0.0750 17.2418 8.800 - 9.000 8.9000 0.0165 0.6745 0.0824 18.5061 9.000 - 9.200 9.1000 0.0096 0.6841 0.0479 10.5381 9.200 - 9.400 9.3000 0.0115 0.6956 0.0574 12.3517 9.400 - 9.600 9.5000 0.0126 0.7082 0.0631 13.2886 9.600 - 9.800 9.7000 0.0060 0.7142 0.0300 6.1882 9.800 - 10.000 9.9000 0.0074 0.7216 0.0369 7.4485 10.000 - 10.200 10.1000 0.0087 0.7303 0.0434 8.5999 10.200 - 10.400 10.3000 0.0037 0.7340 0.0183 3.5625 10.400 - 10.600 10.5000 0.0036 0.7376 0.0180 3.4263 10.600 - 10.800 10.7000 0.0051 0.7426 0.0253 4.7333 10.800 - 11.000 10.9000 0.0051 0.7477 0.0255 4.6703 11.000 - 11.200 11.1000 0.0011 0.7489 0.0057 1.0344 11.200 - 11.400 11.3000 0.0021 0.7510 0.0107 1.8967 11.400 - 11.600 11.5000 0.0037 0.7547 0.0184 3.2052 11.600 - 11.800 11.7000 0.0053 0.7600 0.0263 4.5036 11.800 - 12.000 11.9000 0.0028 0.7628 0.0140 2.3604 12.000 - 12.200 12.1000 -0.0000 0.7628 -0.0000 -0.0000 12.200 - 12.400 12.3000 0.0000 0.7628 0.0000 0.0000 12.400 - 12.600 12.5000 0.0000 0.7628 0.0000 0.0000 12.600 - 12.800 12.7000 -0.0000 0.7628 -0.0000 -0.0000 12.800 - 13.000 12.9000 0.0000 0.7628 0.0000 0.0000 13.000 - 13.200 13.1000 -0.0000 0.7628 -0.0000 -0.0000 13.200 - 13.400 13.3000 0.0000 0.7628 0.0000 0.0000 13.400 - 13.600 13.5000 0.0000 0.7628 0.0000 0.0000 13.600 - 13.800 13.7000 -0.0000 0.7628 -0.0000 -0.0000 13.800 - 14.000 13.9000 0.0000 0.7628 0.0000 0.0000 14.000 - 14.200 14.1000 0.0000 0.7628 0.0000 0.0000 14.200 - 14.400 14.3000 -0.0000 0.7628 -0.0000 -0.0000 14.400 - 14.600 14.5000 0.0000 0.7628 0.0000 0.0000 14.600 - 14.800 14.7000 -0.0000 0.7628 -0.0000 -0.0000 14.800 - 15.000 14.9000 0.0000 0.7628 0.0000 0.0000 15.000 - 15.200 15.1000 0.0000 0.7628 0.0000 0.0000 15.200 - 15.400 15.3000 -0.0000 0.7628 -0.0000 -0.0000 15.400 - 15.600 15.5000 0.0000 0.7628 0.0000 0.0000 15.600 - 15.800 15.7000 -0.0000 0.7628 -0.0000 -0.0000 15.800 - 16.000 15.9000 0.0000 0.7628 0.0000 0.0000 16.000 - 16.200 16.1000 0.0000 0.7628 0.0000 0.0000 16.200 - 16.400 16.3000 -0.0000 0.7628 -0.0000 -0.0000 16.400 - 16.600 16.5000 0.0000 0.7628 0.0000 0.0000 16.600 - 16.800 16.7000 -0.0000 0.7628 -0.0000 -0.0000 16.800 - 17.000 16.9000 0.0000 0.7628 0.0000 0.0000 17.000 - 17.200 17.1000 0.0000 0.7628 0.0000 0.0000 17.200 - 17.400 17.3000 -0.0000 0.7628 -0.0000 -0.0000 17.400 - 17.600 17.5000 0.0000 0.7628 0.0000 0.0000 17.600 - 17.800 17.7000 0.0000 0.7628 0.0000 0.0000 17.800 - 18.000 17.9000 -0.0000 0.7628 -0.0000 -0.0000 18.000 - 18.200 18.1000 0.0000 0.7628 0.0000 0.0000 18.200 - 18.400 18.3000 0.0000 0.7628 0.0000 0.0000 18.400 - 18.600 18.5000 -0.0000 0.7628 -0.0000 -0.0000 18.600 - 18.800 18.7000 0.0000 0.7628 0.0000 0.0000 18.800 - 19.000 18.9000 0.0000 0.7628 0.0000 0.0000 19.000 - 19.200 19.1000 0.0219 0.7847 0.1096 11.4795